Cedren-13-ol, 8-

Base Information

Chemical Name:Cedren-13-ol, 8-
CAS No.:18319-35-2
Molecular Formula:C₁₅H₂₄O
Molecular Weight:220.355
Hs Code.:
Mol file:18319-35-2.mol

Synonyms:1H-3a,7-Methanoazulene-8-methanol,2,3,4,7,8,8a-hexahydro-3,6,8-trimethyl-, [3R-(3a,3ab,7b,8a,8aa)]-; Cedr-8-en-13-ol, (-)- (8CI); 8-Cedren-13-ol

Suppliers and Price of Cedren-13-ol, 8-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of Cedren-13-ol, 8-

Chemical Property:

Boiling Point:306.0±11.0 °C(Predicted)
PKA:14.87±0.10(Predicted)
Density:1.03±0.1 g/cm3(Predicted)

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Cedren-13-ol, 8-

There total 13 articles about Cedren-13-ol, 8- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 118326-12-8
C₁₅H₂₀O₃

: 13836-90-3,18319-31-8,118354-48-6
(+/-)-8,14-Cedranoxide

: 18319-35-2,18319-40-9,118354-44-2
8-cedren-14-ol

Guidance literature:: With potassium hydroxide; hydrazine; In ethylene glycol; for 1.5h; Heating;
DOI:10.1016/S0040-4039(00)96939-9

Reference yield:

: 118343-53-6
Acetic acid (E)-6-(2-hydroxy-4,5-dimethoxy-phenyl)-2-methyl-hept-2-enyl ester

: 18319-35-2,18319-40-9,118354-44-2
8-cedren-14-ol

Guidance literature:: Multi-step reaction with 5 steps

1: (C₄H₉)NBF₄ / acetic acid; acetic anhydride / electrolysis

2: 51 percent / tetrahydrofuran / 2.2 h / -78 °C

3: 93 percent / oxalic acid / methanol / 14 h / Ambient temperature

4: 72 percent / BF₃ etherate / toluene / 2.7 h / Heating

5: 50 percent / KOH/NH₂NH₂ / ethane-1,2-diol / 1.5 h / Heating

With potassium hydroxide; (C₄H₉)NBF₄; boron trifluoride diethyl etherate; oxalic acid; hydrazine; In tetrahydrofuran; methanol; acetic anhydride; ethylene glycol; acetic acid; toluene;
DOI:10.1016/S0040-4039(00)96939-9

Reference yield:

: 118326-11-7
Acetic acid (3R,3aS,6S,8S,8aS)-6-hydroxy-3,6,8-trimethyl-5,9-dioxo-octahydro-3a,7-methano-azulen-8-ylmethyl ester

: 18319-35-2,18319-40-9,118354-44-2
8-cedren-14-ol

Guidance literature:: Multi-step reaction with 2 steps

1: 72 percent / BF₃ etherate / toluene / 2.7 h / Heating

2: 50 percent / KOH/NH₂NH₂ / ethane-1,2-diol / 1.5 h / Heating

With potassium hydroxide; boron trifluoride diethyl etherate; hydrazine; In ethylene glycol; toluene;
DOI:10.1016/S0040-4039(00)96939-9