methoxo(2,3,6,7,12,13-hexabromo-5,10,15-tri(4-tert-butylphenyl)subporphyrinate)boron(III)

Base Information

• Chemical Name: methoxo(2,3,6,7,12,13-hexabromo-5,10,15-tri(4-tert-butylphenyl)subporphyrinate)boron(III)
• CAS No.: 1318254-59-9
• Molecular Formula: C₄₆H₄₂BBr₆N₃O
• Molecular Weight: 1143.09
• Mol file: 1318254-59-9.mol

Synonyms:methoxo(2,3,6,7,12,13-hexabromo-5,10,15-tri(4-tert-butylphenyl)subporphyrinate)boron(III)

Chemical Property of methoxo(2,3,6,7,12,13-hexabromo-5,10,15-tri(4-tert-butylphenyl)subporphyrinate)boron(III)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of methoxo(2,3,6,7,12,13-hexabromo-5,10,15-tri(4-tert-butylphenyl)subporphyrinate)boron(III)

There total 1 articles about methoxo(2,3,6,7,12,13-hexabromo-5,10,15-tri(4-tert-butylphenyl)subporphyrinate)boron(III) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

methoxo(5,10,15-tri(4-tert-butylphenyl)subporphyrinato)boron(III) → methoxo(2,3,6,7,12,13-hexabromo-5,10,15-tri(4-tert-butylphenyl)subporphyrinate)boron(III) (1318254-59-9)

Guidance literature:

With bromine; In chloroform; at 20 ℃; for 2h; Inert atmosphere;

DOI:10.1021/ja2056566

Reference yield: 62.0%

Et3Si+[CHB11H5Br6]- + methoxo(2,3,6,7,12,13-hexabromo-5,10,15-tri(4-tert-butylphenyl)subporphyrinate)boron(III) (1318254-59-9) → (B(N3C15Br6(C6H4C(CH3)3)3))(1+)*HCB11H5Br6(1-)=(B(N3C15Br6(C6H4C(CH3)3)3))(HCB11H5Br6)

Guidance literature:

In toluene; room temp., 3 h; ppt. was filtered;

DOI:10.1021/ja2056566