1-(2-(4-chlorobenzyloxy)-2-(2,4-dichlorophenyl)ethyl)-1H-benzo[d][1,2,3]triazole

Base Information

Chemical Name:1-(2-(4-chlorobenzyloxy)-2-(2,4-dichlorophenyl)ethyl)-1H-benzo[d][1,2,3]triazole
CAS No.:1301629-05-9
Molecular Formula:C₂₁H₁₆Cl₃N₃O
Molecular Weight:432.737
Hs Code.:

Synonyms:1-(2-(4-chlorobenzyloxy)-2-(2,4-dichlorophenyl)ethyl)-1H-benzo[d][1,2,3]triazole

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Chemical Property of 1-(2-(4-chlorobenzyloxy)-2-(2,4-dichlorophenyl)ethyl)-1H-benzo[d][1,2,3]triazole

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Technology Process of 1-(2-(4-chlorobenzyloxy)-2-(2,4-dichlorophenyl)ethyl)-1H-benzo[d][1,2,3]triazole

There total 2 articles about 1-(2-(4-chlorobenzyloxy)-2-(2,4-dichlorophenyl)ethyl)-1H-benzo[d][1,2,3]triazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 163729-38-2
2-(1H-benzo[d][1,2,3]triazol-1-yl)-1-(2,4-dichlorophenyl)ethanol

: 622-95-7
4-chlorobenzyl bromide

: 1301629-05-9
1-(2-(4-chlorobenzyloxy)-2-(2,4-dichlorophenyl)ethyl)-1H-benzo[d][1,2,3]triazole

Guidance literature:: With tetra-(n-butyl)ammonium iodide; sodium hydride; In N,N-dimethyl-formamide; at -78 - 20 ℃; for 2h; Inert atmosphere;
DOI:10.1016/j.bmcl.2012.09.041

Reference yield:

: 13692-14-3,114446-57-0
α-(chloromethyl)-2,4-dichlorobenzyl alcohol

: 273-02-9
2H-benzo[d][1,2,3]triazole

: 1301629-05-9
1-(2-(4-chlorobenzyloxy)-2-(2,4-dichlorophenyl)ethyl)-1H-benzo[d][1,2,3]triazole

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / acetonitrile / 0.83 h / 80 °C / Microwave irradiation

2: tetra-(n-butyl)ammonium iodide; sodium hydride / N,N-dimethyl-formamide / 2 h / -78 - 20 °C / Inert atmosphere

With tetra-(n-butyl)ammonium iodide; sodium hydride; potassium carbonate; In N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/j.bmcl.2012.09.041