4-(2,6-dioxo-1-prop-2-ynyl-2,3,6,7-tetrahydro-1H-purin-8-yl)benzenesulfonic acid 4-nitrophenyl ester

Base Information

Chemical Name:4-(2,6-dioxo-1-prop-2-ynyl-2,3,6,7-tetrahydro-1H-purin-8-yl)benzenesulfonic acid 4-nitrophenyl ester
CAS No.:1161743-38-9
Molecular Formula:C₂₀H₁₃N₅O₇S
Molecular Weight:467.419
Hs Code.:

Synonyms:4-(2,6-dioxo-1-prop-2-ynyl-2,3,6,7-tetrahydro-1H-purin-8-yl)benzenesulfonic acid 4-nitrophenyl ester

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Chemical Property of 4-(2,6-dioxo-1-prop-2-ynyl-2,3,6,7-tetrahydro-1H-purin-8-yl)benzenesulfonic acid 4-nitrophenyl ester

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Technology Process of 4-(2,6-dioxo-1-prop-2-ynyl-2,3,6,7-tetrahydro-1H-purin-8-yl)benzenesulfonic acid 4-nitrophenyl ester

There total 1 articles about 4-(2,6-dioxo-1-prop-2-ynyl-2,3,6,7-tetrahydro-1H-purin-8-yl)benzenesulfonic acid 4-nitrophenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.9%

: 1161743-36-7
4-(6-amino-2,4-dioxo-3-prop-2-ynyl-1,2,3,4-tetrahydropyrimidin-5-ylcarbamoyl)benzenesulfonic acid 4-nitrophenyl ester

: 1161743-38-9
4-(2,6-dioxo-1-prop-2-ynyl-2,3,6,7-tetrahydro-1H-purin-8-yl)benzenesulfonic acid 4-nitrophenyl ester

Guidance literature:: With ammonium sulfate; 1,1,1,3,3,3-hexamethyl-disilazane; for 16h; Reflux;
DOI:10.1021/jm900413e

Reference yield: 38.0%

: 38212-33-8
4-(4-chlorophenyl) piperazine

: 1161743-38-9
4-(2,6-dioxo-1-prop-2-ynyl-2,3,6,7-tetrahydro-1H-purin-8-yl)benzenesulfonic acid 4-nitrophenyl ester

: 1161743-64-1
8-(4-(4-(4-chlorophenyl)piperazine-1-sulfonyl)phenyl)-1-prop-2-ynyl-3,7-dihydropurine-2,6-dione

Guidance literature:: 4-(4-chlorophenyl) piperazine; 4-(2,6-dioxo-1-prop-2-ynyl-2,3,6,7-tetrahydro-1H-purin-8-yl)benzenesulfonic acid 4-nitrophenyl ester; In N,N-dimethyl-formamide; at 20 ℃; for 48h;

With ammonium hydroxide; water; at 60 ℃; for 0.333333h; pH=11;
DOI:10.1021/jm900413e