1-(2-HYDROXYPHENYL)PROPAN-1-ONE OXIME

Base Information

• Chemical Name: 1-(2-HYDROXYPHENYL)PROPAN-1-ONE OXIME
• CAS No.: 18265-75-3
• Molecular Formula: C9H11 N O2
• Molecular Weight: 165.192
• Hs Code.: 2928000090
• Mol file: 18265-75-3.mol

Synonyms:Propiophenone,2'-hydroxy-, oxime (8CI); 2'-Hydroxypropiophenone oxime; Ethyl o-hydroxyphenylketone oxime; o-Hydroxypropiophenone, oxime; o-Hydroxypropiophenoxime

Chemical Property of 1-(2-HYDROXYPHENYL)PROPAN-1-ONE OXIME

Chemical Property:

• PSA: 49.33000
• LogP: 1.71530

Purity/Quality:

99%, ^*data from raw suppliers

1-(2-hydroxyphenyl)propan-1-oneoxime 95% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-(2-HYDROXYPHENYL)PROPAN-1-ONE OXIME

There total 1 articles about 1-(2-HYDROXYPHENYL)PROPAN-1-ONE OXIME which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

1-(2-Hydroxy-phenyl)-propan-1-on (610-99-1) → 1-(2-hydroxy-phenyl)-propan-1-one oxime (18265-75-3)

Guidance literature:

With hydroxylamine hydrochloride; sodium acetate; In ethanol; for 2.5h; Heating;

DOI:10.1021/jm020581y

Reference yield: 92.0%

1-(2-hydroxy-phenyl)-propan-1-one oxime (18265-75-3) → 2-ethyl-1,3-benzoxazole (6797-13-3)

Guidance literature:

With HY-Zeolite; In benzene; at 160 ℃; for 168h;

DOI:10.1080/00397919508013850

Reference yield: 89.0%

1-(2-hydroxy-phenyl)-propan-1-one oxime (18265-75-3) + acetic anhydride (108-24-7) → 1-(2-hydroxyphenyl)propan-1-one O-acetyloxime

Guidance literature:

for 0.166667h;

DOI:10.1021/jm020581y

upstream raw materials:

1-(2-Hydroxy-phenyl)-propan-1-on

Downstream raw materials:

3-ethyl-1,2-benzisoxazole 2-oxide

2-ethyl-1,3-benzoxazole

[Cu(S₂CN(CH₂C₆H₅)2)(OC₆H₄C(CH₂CH₃)(NOH))]

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