phenyl N-[4-(4-amino-3-fluorophenoxy)pyridin-2-yl]-N-phenoxycarbonylcarbamate

Base Information

Chemical Name:phenyl N-[4-(4-amino-3-fluorophenoxy)pyridin-2-yl]-N-phenoxycarbonylcarbamate
CAS No.:928038-53-3
Molecular Formula:C₂₅H₁₈FN₃O₅
Molecular Weight:459.433
Hs Code.:

Synonyms:phenyl N-[4-(4-amino-3-fluorophenoxy)pyridin-2-yl]-N-phenoxycarbonylcarbamate

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Chemical Property of phenyl N-[4-(4-amino-3-fluorophenoxy)pyridin-2-yl]-N-phenoxycarbonylcarbamate

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Technology Process of phenyl N-[4-(4-amino-3-fluorophenoxy)pyridin-2-yl]-N-phenoxycarbonylcarbamate

There total 5 articles about phenyl N-[4-(4-amino-3-fluorophenoxy)pyridin-2-yl]-N-phenoxycarbonylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 928038-52-2
phenyl N-[4-(4-benzyloxycarbonylamino-3-fluorophenoxy)pyridin-2-yl]-N-phenoxycarbonylcarbamate

: 928038-53-3
phenyl N-[4-(4-amino-3-fluorophenoxy)pyridin-2-yl]-N-phenoxycarbonylcarbamate

Guidance literature:: With hydrogen; 20% Pd(OH)2/C; In tetrahydrofuran; at 20 ℃; for 4h;

Reference yield:

: 864245-68-1
benzyl (4-((2-aminopyridin-4-yl)oxy)-2-fluorophenyl)carbamate

: 928038-53-3
phenyl N-[4-(4-amino-3-fluorophenoxy)pyridin-2-yl]-N-phenoxycarbonylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / tetrahydrofuran / 1 h / 20 °C

2: hydrogen / palladium(II) hydroxide/carbon / tetrahydrofuran / 4 h / 20 °C

With hydrogen; triethylamine; palladium(II) hydroxide/carbon; In tetrahydrofuran;

Reference yield:

: 864245-67-0
4-(4-benzyloxycarbonylamino-3-fluorophenoxy)pyridine-2-carboxylic acid

: 928038-53-3
phenyl N-[4-(4-amino-3-fluorophenoxy)pyridin-2-yl]-N-phenoxycarbonylcarbamate

Guidance literature:: Multi-step reaction with 4 steps

1: diphenyl phosphoryl azide; triethylamine / 5 h / 20 - 100 °C

2: hydrogenchloride / ethyl acetate / 3.67 h / 0 - 20 °C

3: triethylamine / tetrahydrofuran / 1 h / 20 °C

4: hydrogen / palladium(II) hydroxide/carbon / tetrahydrofuran / 4 h / 20 °C

With hydrogenchloride; diphenyl phosphoryl azide; hydrogen; triethylamine; palladium(II) hydroxide/carbon; In tetrahydrofuran; ethyl acetate;