9-(6-(4-(5-(4-tert-butylphenyl)-1,3,4-oxadiazol-2-yl)phenoxy)hexyl)-9H-carbazole

Base Information

• Chemical Name: 9-(6-(4-(5-(4-tert-butylphenyl)-1,3,4-oxadiazol-2-yl)phenoxy)hexyl)-9H-carbazole
• CAS No.: 1252660-24-4
• Molecular Formula: C₃₆H₃₇N₃O₂
• Molecular Weight: 543.709
• Mol file: 1252660-24-4.mol

Synonyms:9-(6-(4-(5-(4-tert-butylphenyl)-1,3,4-oxadiazol-2-yl)phenoxy)hexyl)-9H-carbazole

Chemical Property of 9-(6-(4-(5-(4-tert-butylphenyl)-1,3,4-oxadiazol-2-yl)phenoxy)hexyl)-9H-carbazole

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 9-(6-(4-(5-(4-tert-butylphenyl)-1,3,4-oxadiazol-2-yl)phenoxy)hexyl)-9H-carbazole

There total 1 articles about 9-(6-(4-(5-(4-tert-butylphenyl)-1,3,4-oxadiazol-2-yl)phenoxy)hexyl)-9H-carbazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

2-(4-hydroxyphenyl)-5-(4-tert-butylphenyl)-1,3,4-oxadiazole (292869-69-3) + N-(6-bromohexyl)carbazole (94847-10-6) → 9-(6-(4-(5-(4-tert-butylphenyl)-1,3,4-oxadiazol-2-yl)phenoxy)hexyl)-9H-carbazole (1252660-24-4)

Guidance literature:

With potassium carbonate; potassium iodide; In N,N-dimethyl-formamide; at 100 ℃; for 24h; Inert atmosphere;

DOI:10.1016/j.dyepig.2012.05.015

Reference yield: 45.0%

9-(6-(4-(5-(4-tert-butylphenyl)-1,3,4-oxadiazol-2-yl)phenoxy)hexyl)-9H-carbazole (1252660-24-4) + N,N-dimethyl-formamide (68-12-2,33513-42-7) → 9-(6-(4-(5-(4-tert-butylphenyl)-1,3,4-oxadiazol-2-yl)phenoxy)hexyl)-9H-carbazole-3,6-dicarbaldehyde (1402660-07-4)

Guidance literature:

With trichlorophosphate; In 1,2-dichloro-ethane; at 0 - 90 ℃; for 48h;

DOI:10.1016/j.dyepig.2012.05.015

Reference yield:

9-(6-(4-(5-(4-tert-butylphenyl)-1,3,4-oxadiazol-2-yl)phenoxy)hexyl)-9H-carbazole (1252660-24-4) → C62H51N9O2 (1402660-11-0)

Guidance literature:

Multi-step reaction with 2 steps

1.1: trichlorophosphate / 1,2-dichloro-ethane / 48 h / 0 - 90 °C

2.1: acetic acid / chloroform / 0.33 h

2.2: 24 h / Inert atmosphere; Reflux

With acetic acid; trichlorophosphate; In chloroform; 1,2-dichloro-ethane;

DOI:10.1016/j.dyepig.2012.05.015

upstream raw materials:

2-(4-hydroxyphenyl)-5-(4-tert-butylphenyl)-1,3,4-oxadiazole

N-(6-bromohexyl)carbazole

Downstream raw materials:

C₆₂H₅₁N₉O₂

9-(6-(4-(5-(4-tert-butylphenyl)-1,3,4-oxadiazol-2-yl)phenoxy)hexyl)-9H-carbazole-3,6-dicarbaldehyde