(3S,4R,4'R,5'R)-4-[4',5'-bis(methoxydiphenylmethyl)-1',3',2'-dioxaborolan-2'-yl]-1-phenylhex-5-en-3-ol

Base Information

Chemical Name:(3S,4R,4'R,5'R)-4-[4',5'-bis(methoxydiphenylmethyl)-1',3',2'-dioxaborolan-2'-yl]-1-phenylhex-5-en-3-ol
CAS No.:1178609-30-7
Molecular Formula:C₄₂H₄₃BO₅
Molecular Weight:638.611
Hs Code.:

Synonyms:(3S,4R,4'R,5'R)-4-[4',5'-bis(methoxydiphenylmethyl)-1',3',2'-dioxaborolan-2'-yl]-1-phenylhex-5-en-3-ol

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Chemical Property of (3S,4R,4'R,5'R)-4-[4',5'-bis(methoxydiphenylmethyl)-1',3',2'-dioxaborolan-2'-yl]-1-phenylhex-5-en-3-ol

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Technology Process of (3S,4R,4'R,5'R)-4-[4',5'-bis(methoxydiphenylmethyl)-1',3',2'-dioxaborolan-2'-yl]-1-phenylhex-5-en-3-ol

There total 3 articles about (3S,4R,4'R,5'R)-4-[4',5'-bis(methoxydiphenylmethyl)-1',3',2'-dioxaborolan-2'-yl]-1-phenylhex-5-en-3-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 104-53-0
3-phenyl-propionaldehyde

: 1240510-17-1
(4'R,5'R,2E)-3-[4',5'-bis(methoxydiphenylmethyl)-1',3',2'-dioxaborolan-2'-yl]prop-2-en-1-yl methanesulfonate

: 1178609-30-7
(3S,4R,4'R,5'R)-4-[4',5'-bis(methoxydiphenylmethyl)-1',3',2'-dioxaborolan-2'-yl]-1-phenylhex-5-en-3-ol

: (3S,4S,4'R,5'R)-4-[4',5'-bis(methoxydiphenylmethyl)-1',3',2'-dioxaborolan-2'-yl]-1-phenylhex-5-en-3-ol

: (3S,4R,4'R,5'R)-4-[4',5'-bis(methoxydiphenylmethyl)-1',3',2'-dioxaborolan-2'-yl]-1-phenylhex-5-en-3-ol

Guidance literature:: With bis(benzonitrile)palladium(II) dichloride; water; tin(ll) chloride; In N,N-dimethyl-formamide; at 20 ℃; diastereoselective reaction; Inert atmosphere;
DOI:10.1021/jo1008959

Reference yield:

: 104-53-0
3-phenyl-propionaldehyde

: C₃₉H₄₇BO₅Si

: 1178609-30-7
(3S,4R,4'R,5'R)-4-[4',5'-bis(methoxydiphenylmethyl)-1',3',2'-dioxaborolan-2'-yl]-1-phenylhex-5-en-3-ol

: C₄₂H₄₃BO₅

Guidance literature:: C₃₉H₄₇BO₅Si; With tetrahydroxydiboron; In dimethyl sulfoxide; acetonitrile; at 20 ℃;

3-phenyl-propionaldehyde; With tetrakis(acetonitrile)palladium(II) tetrafluoroborate; toluene-4-sulfonic acid; In dimethyl sulfoxide; acetonitrile; at 6 ℃; for 18h; Overall yield = 90 %; diastereoselective reaction;
DOI:10.1021/jo5004168

Reference yield:

: 104-53-0
3-phenyl-propionaldehyde

: 1240510-17-1
(4'R,5'R,2E)-3-[4',5'-bis(methoxydiphenylmethyl)-1',3',2'-dioxaborolan-2'-yl]prop-2-en-1-yl methanesulfonate

: 1178609-30-7
(3S,4R,4'R,5'R)-4-[4',5'-bis(methoxydiphenylmethyl)-1',3',2'-dioxaborolan-2'-yl]-1-phenylhex-5-en-3-ol

: (3S,4S,4'R,5'R)-4-[4',5'-bis(methoxydiphenylmethyl)-1',3',2'-dioxaborolan-2'-yl]-1-phenylhex-5-en-3-ol

: C₄₂H₄₃BO₅

Guidance literature:: With cis-dichlorobis(benzonitrile)palladium(II); tin(ll) chloride; In water; N,N-dimethyl-formamide; at 20 ℃; for 2h; diastereoselective reaction;
DOI:10.1055/s-0029-1217160