dibenzylphosphoryl 3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

Base Information

• Chemical Name: dibenzylphosphoryl 3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranoside
• CAS No.: 88862-86-6
• Molecular Formula: C₃₄H₃₄NO₁₃P
• Molecular Weight: 695.617

Synonyms:dibenzylphosphoryl 3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

Chemical Property of dibenzylphosphoryl 3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

Chemical Property:

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Technology Process of dibenzylphosphoryl 3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

There total 4 articles about dibenzylphosphoryl 3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

phosphoric acid dibenzyl ester (1623-08-1) + 3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-D-glucopyranose (72858-55-0,90405-21-3,90405-42-8,124362-60-3,144221-86-3) → dibenzylphosphoryl 3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranoside (88862-86-6)

Guidance literature:

3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-D-glucopyranose; With Dibenzothiophene sulfoxide; 2,4,6-tri-tertbutylpyridine; trifluoromethylsulfonic anhydride; In dichloromethane; at -45 ℃; for 1h;

phosphoric acid dibenzyl ester; In dichloromethane; at -45 - 23 ℃; Further stages.;

DOI:10.1021/ol006041h

Reference yield: 71.0%

phosphoric acid dibenzyl ester (1623-08-1) + 4'-pentenyl 2-N-phthalimido-3,4,6-tri-O-acetylglucoside (124771-17-1) → dibenzylphosphoryl 3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranoside (88862-86-6)

Guidance literature:

With N-Bromosuccinimide; In acetonitrile; for 11h; Ambient temperature;

DOI:10.1021/jo00014a043

Reference yield:

→ dibenzylphosphoryl 3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranoside (88862-86-6)

Guidance literature:

3,4,6-Tri-O-acetyl-1-chlor-2-desoxy-2-phthalimido-β-D-glucose, Ag-Dibenzylphosphat, in sd. Bzl.;

upstream raw materials:

phosphoric acid dibenzyl ester

4'-pentenyl 2-N-phthalimido-3,4,6-tri-O-acetylglucoside

3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-D-glucopyranose

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