12,12-Bis-benzenesulfonyl-15-(tert-butyl-dimethyl-silanyloxy)-pentadecanoic acid methyl ester

Base Information

Chemical Name:12,12-Bis-benzenesulfonyl-15-(tert-butyl-dimethyl-silanyloxy)-pentadecanoic acid methyl ester
CAS No.:121942-39-0
Molecular Formula:C₃₄H₅₄O₇S₂Si
Molecular Weight:667.016
Hs Code.:

Synonyms:12,12-Bis-benzenesulfonyl-15-(tert-butyl-dimethyl-silanyloxy)-pentadecanoic acid methyl ester

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Chemical Property of 12,12-Bis-benzenesulfonyl-15-(tert-butyl-dimethyl-silanyloxy)-pentadecanoic acid methyl ester

Chemical Property:

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Technology Process of 12,12-Bis-benzenesulfonyl-15-(tert-butyl-dimethyl-silanyloxy)-pentadecanoic acid methyl ester

There total 7 articles about 12,12-Bis-benzenesulfonyl-15-(tert-butyl-dimethyl-silanyloxy)-pentadecanoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 89031-84-5
3-(tert-butyldimethylsilyloxy)propyl bromide

: 121942-38-9
12,12-Bis-benzenesulfonyl-dodecanoic acid methyl ester

: 121942-39-0
12,12-Bis-benzenesulfonyl-15-(tert-butyl-dimethyl-silanyloxy)-pentadecanoic acid methyl ester

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; 1) r.t., 1 h, 2) 80 deg C, 7 h;

Reference yield:

: 2834-05-1
11-bromoundecanoic acid

: 121942-39-0
12,12-Bis-benzenesulfonyl-15-(tert-butyl-dimethyl-silanyloxy)-pentadecanoic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: diethyl ether

2: 1) NaH / 1.) DMF, r.t., 1 h, 2) DMF, 80 deg C, 7 h

3: 92 percent / 1) NaH / dimethylformamide / 1) r.t., 1 h, 2) 80 deg C, 7 h

With sodium hydride; In diethyl ether; N,N-dimethyl-formamide;

Reference yield:

: 6287-90-7
11-bromo-undecanoic acid methyl ester

: 121942-39-0
12,12-Bis-benzenesulfonyl-15-(tert-butyl-dimethyl-silanyloxy)-pentadecanoic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1) NaH / 1.) DMF, r.t., 1 h, 2) DMF, 80 deg C, 7 h

2: 92 percent / 1) NaH / dimethylformamide / 1) r.t., 1 h, 2) 80 deg C, 7 h

With sodium hydride; In N,N-dimethyl-formamide;