C₆₄H₁₁₅O₁₄PSi₃

Base Information

Chemical Name:C₆₄H₁₁₅O₁₄PSi₃
CAS No.:1422462-97-2
Molecular Formula:C₆₄H₁₁₅O₁₄PSi₃
Molecular Weight:1223.84
Hs Code.:

C<sub>64</sub>H<sub>115</sub>O<sub>14</sub>PSi<sub>3</sub>

Synonyms:C₆₄H₁₁₅O₁₄PSi₃

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₆₄H₁₁₅O₁₄PSi₃

Chemical Property:

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Technology Process of C₆₄H₁₁₅O₁₄PSi₃

There total 30 articles about C₆₄H₁₁₅O₁₄PSi₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 1033588-04-3
C₁₃H₂₃O₆P

: 1422462-95-0
C₅₁H₉₄O₉Si₃

: 1422462-97-2
C₆₄H₁₁₅O₁₄PSi₃

Guidance literature:: C₁₃H₂₃O₆P; With 2,4,6-trichlorobenzoyl chloride; triethylamine; In toluene; at 20 ℃; for 6h; Inert atmosphere;

C₅₁H₉₄O₉Si₃; With dmap; In toluene; at 20 ℃; for 16h; Inert atmosphere;
DOI:10.1021/jo3026077

Reference yield:

: 1422462-85-8
C₂₆H₄₈O₅Si₂

: 1422462-97-2
C₆₄H₁₁₅O₁₄PSi₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: lithium diisopropyl amide / tetrahydrofuran; diethyl ether / 0.33 h / -78 °C / Inert atmosphere

1.2: 0.33 h / -78 °C / Inert atmosphere

2.1: triethylamine / dichloromethane / 0.33 h / -78 °C / Inert atmosphere

3.1: water; acetic acid / tetrahydrofuran / 0.67 h / 0 °C

4.1: 2,4,6-trichlorobenzoyl chloride; triethylamine / toluene / 6 h / 20 °C / Inert atmosphere

4.2: 16 h / 20 °C / Inert atmosphere

With 2,4,6-trichlorobenzoyl chloride; water; acetic acid; triethylamine; lithium diisopropyl amide; In tetrahydrofuran; diethyl ether; dichloromethane; toluene;
DOI:10.1021/jo3026077

Reference yield:

: C₂₉H₄₈O₅Si

: 1422462-97-2
C₆₄H₁₁₅O₁₄PSi₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: water; sodium periodate / tetrahydrofuran; diethyl ether / 2 h / 20 °C

2.1: lithium diisopropyl amide / tetrahydrofuran; diethyl ether / 0.33 h / -78 °C / Inert atmosphere

2.2: 0.33 h / -78 °C / Inert atmosphere

3.1: triethylamine / dichloromethane / 0.33 h / -78 °C / Inert atmosphere

4.1: water; acetic acid / tetrahydrofuran / 0.67 h / 0 °C

5.1: 2,4,6-trichlorobenzoyl chloride; triethylamine / toluene / 6 h / 20 °C / Inert atmosphere

5.2: 16 h / 20 °C / Inert atmosphere

With sodium periodate; 2,4,6-trichlorobenzoyl chloride; water; acetic acid; triethylamine; lithium diisopropyl amide; In tetrahydrofuran; diethyl ether; dichloromethane; toluene;
DOI:10.1021/jo3026077