(1'R,2'S,5'R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl 2-benzoylacrylate

Base Information

Chemical Name:(1'R,2'S,5'R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl 2-benzoylacrylate
CAS No.:115704-79-5
Molecular Formula:C₂₆H₃₀O₃
Molecular Weight:390.522
Hs Code.:

Synonyms:(1'R,2'S,5'R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl 2-benzoylacrylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1'R,2'S,5'R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl 2-benzoylacrylate

Chemical Property:

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Technology Process of (1'R,2'S,5'R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl 2-benzoylacrylate

There total 7 articles about (1'R,2'S,5'R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl 2-benzoylacrylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 175849-28-2
(1'R,2'S,5'R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl 2-<(methylsulfinyl)methyl>-3-oxo-3-phenylpropionate

: 115704-79-5
(1'R,2'S,5'R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl 2-benzoylacrylate

Guidance literature:: In toluene; for 12h; Heating;
DOI:10.1021/jo9518819

Reference yield:

: 65253-04-5
(-)-8-phenylmenthol

: 115704-79-5
(1'R,2'S,5'R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl 2-benzoylacrylate

Guidance literature:: Multi-step reaction with 5 steps

1: 83 percent / Et₃N, DMAP / CH₂Cl₂ / 10 h / Ambient temperature

2: 97 percent / 10percent HCl / methanol / 12 h / Ambient temperature

3: 96 percent / dioxane / 17 h / 90 °C

4: 92 percent / NaIO₄ / methanol; H₂O / 12 h / Ambient temperature

5: 97 percent / toluene / 12 h / Heating

With hydrogenchloride; dmap; sodium periodate; triethylamine; In 1,4-dioxane; methanol; dichloromethane; water; toluene;
DOI:10.1021/jo9518819

Reference yield:

: 85892-91-7
2-(2-phenyl-1,3-dioxolan-2-yl)acetic acid

: 115704-79-5
(1'R,2'S,5'R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl 2-benzoylacrylate

Guidance literature:: Multi-step reaction with 6 steps

1: (COCl)2 / benzene / 3 h / Ambient temperature

2: 83 percent / Et₃N, DMAP / CH₂Cl₂ / 10 h / Ambient temperature

3: 97 percent / 10percent HCl / methanol / 12 h / Ambient temperature

4: 96 percent / dioxane / 17 h / 90 °C

5: 92 percent / NaIO₄ / methanol; H₂O / 12 h / Ambient temperature

6: 97 percent / toluene / 12 h / Heating

With hydrogenchloride; dmap; sodium periodate; oxalyl dichloride; triethylamine; In 1,4-dioxane; methanol; dichloromethane; water; toluene; benzene;
DOI:10.1021/jo9518819