4'-DECYLOXYACETOPHENONE

Base Information

• Chemical Name: 4'-DECYLOXYACETOPHENONE
• CAS No.: 18099-59-7
• Molecular Formula: C18H28O2
• Molecular Weight: 276.419
• Hs Code.: 2914509090
• Mol file: 18099-59-7.mol

Synonyms:4'-(Decyloxy)acetophenone;p-Decyloxyacetophenone;1-(4-((Decyl)oxy)phenyl)ethanone;4-Decyloxyacetophenone;Acetophenone,4'-(decyloxy)- (8CI);

Chemical Property of 4'-DECYLOXYACETOPHENONE

Chemical Property:

• Appearance/Colour: white flakes
• Melting Point: 35-37 °C
• Refractive Index: 1.5510 (estimate)
• Boiling Point: 394.3 °C at 760 mmHg
• Flash Point: 154.3 °C
• PSA: 26.30000
• Density: 0.941 g/cm³
• LogP: 5.40870

Purity/Quality:

98%min ^*data from raw suppliers

1-(4-(Decyloxy)phenyl)ethanone 95+% ^*data from reagent suppliers

Safty Information:

• Safety Statements: 24/25

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4'-DECYLOXYACETOPHENONE

There total 4 articles about 4'-DECYLOXYACETOPHENONE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.3%

sodium hydroxide (1310-73-2) + 1-bromo dodecane (112-29-8) + 4-Hydroxyacetophenone (99-93-4) → 4-decyloxyacetophenone (18099-59-7)

Guidance literature:

In N,N-dimethyl-formamide;

Reference yield: 89.0%

1-bromo dodecane (112-29-8) + 4-Hydroxyacetophenone (99-93-4) → 4-decyloxyacetophenone (18099-59-7)

Guidance literature:

With tetra-(n-butyl)ammonium iodide; In butanone; for 5h; Reflux;

DOI:10.1139/V10-057

Reference yield: 68.0%

4-Hydroxyacetophenone (99-93-4) → 4-decyloxyacetophenone (18099-59-7)

Guidance literature:

With potassium carbonate; potassium iodide; In ethanol; for 35h; Heating;

DOI:10.1007/BF00703490

upstream raw materials:

1-bromo dodecane

4-Hydroxyacetophenone

sodium hydroxide

Downstream raw materials:

(E)-1,3-Bis-(4-decyloxy-phenyl)-propenone

1,3-bis(4-decyloxyphenyl)propane-1,3-dione

α-bromomethyl p(n-dicyloxy)phenyl cetone

2-(4-decyloxybenzoyl)allyldimethylamine

Refernces

• 1、 Lei, Zih-Yang,Lee, Gene-Hsiang,Lai, Chung K.. "Luminescent mesogenic borondifluoride complexes with the Schiff bases containing salicylideneamines and β-enaminoketones core systems". . p. 44 - 56. Retrieved 2018/04/02.
• 2、 Sowmya,Rai, K. M. Lokanatha. "Synthesis and liquid crystalline properties of a new homologous series of 4,5-disubstituted 2H-[1,2,3]-triazoles via azide-chalcone oxidative cycloaddition reaction". . p. 764 - 768. Retrieved 2017/07/07.