N-Bicyclo[5.3.1]undec-1⁽¹⁰⁾-en-(9E)-ylidene-N'-(2,4-dinitro-phenyl)-hydrazine

Base Information

Chemical Name:N-Bicyclo[5.3.1]undec-1⁽¹⁰⁾-en-(9E)-ylidene-N'-(2,4-dinitro-phenyl)-hydrazine
CAS No.:73274-46-1
Molecular Formula:C₁₇H₂₀N₄O₄
Molecular Weight:344.37
Hs Code.:

N-Bicyclo[5.3.1]undec-1<sup>(10)</sup>-en-(9E)-ylidene-N'-(2,4-dinitro-phenyl)-hydrazine

Synonyms:N-Bicyclo[5.3.1]undec-1⁽¹⁰⁾-en-(9E)-ylidene-N'-(2,4-dinitro-phenyl)-hydrazine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-Bicyclo[5.3.1]undec-1⁽¹⁰⁾-en-(9E)-ylidene-N'-(2,4-dinitro-phenyl)-hydrazine

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Technology Process of N-Bicyclo[5.3.1]undec-1⁽¹⁰⁾-en-(9E)-ylidene-N'-(2,4-dinitro-phenyl)-hydrazine

There total 3 articles about N-Bicyclo[5.3.1]undec-1⁽¹⁰⁾-en-(9E)-ylidene-N'-(2,4-dinitro-phenyl)-hydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 73274-32-5
Bicyclo [5.3.1]undec-10-en-9-one

: 119-26-6
(2,4-dinitro-phenyl)-hydrazine

: 73274-46-1
N-Bicyclo[5.3.1]undec-1⁽¹⁰⁾-en-(9E)-ylidene-N'-(2,4-dinitro-phenyl)-hydrazine

Guidance literature:: With hydrogenchloride; In ethanol; Heating;
DOI:10.1021/jo01298a012

Reference yield:

: 23202-10-0
(Z)-cyclooct-2-enone

: 73274-46-1
N-Bicyclo[5.3.1]undec-1⁽¹⁰⁾-en-(9E)-ylidene-N'-(2,4-dinitro-phenyl)-hydrazine

Guidance literature:: Multi-step reaction with 3 steps

1: 68 percent / NaOEt / ethanol / 14 h / 25 °C

2: 29 percent / H₂SO₄ / acetic acid; H₂O / 5 h / Heating

3: 98 percent / aq. HCl / ethanol / Heating

With hydrogenchloride; sulfuric acid; sodium ethanolate; In ethanol; water; acetic acid;
DOI:10.1021/jo01298a012

Reference yield:

: 77188-48-8
ethyl 2-(3-oxocyclo-octyl)acetoacetate

: 73274-46-1
N-Bicyclo[5.3.1]undec-1⁽¹⁰⁾-en-(9E)-ylidene-N'-(2,4-dinitro-phenyl)-hydrazine

Guidance literature:: Multi-step reaction with 2 steps

1: 29 percent / H₂SO₄ / acetic acid; H₂O / 5 h / Heating

2: 98 percent / aq. HCl / ethanol / Heating

With hydrogenchloride; sulfuric acid; In ethanol; water; acetic acid;
DOI:10.1021/jo01298a012