O³-benzyl-O¹,O²-isopropylidene-O⁵,O⁶-bis-methanesulfonyl-α-D-allofuranose

Base Information

• Chemical Name: O³-benzyl-O¹,O²-isopropylidene-O⁵,O⁶-bis-methanesulfonyl-α-D-allofuranose
• CAS No.: 22331-20-0
• Molecular Formula: C₁₈H₂₆O₁₀S₂
• Molecular Weight: 466.53

Synonyms:O³-benzyl-O¹,O²-isopropylidene-O⁵,O⁶-bis-methanesulfonyl-α-D-allofuranose

Chemical Property of O³-benzyl-O¹,O²-isopropylidene-O⁵,O⁶-bis-methanesulfonyl-α-D-allofuranose

Chemical Property:

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Technology Process of O³-benzyl-O¹,O²-isopropylidene-O⁵,O⁶-bis-methanesulfonyl-α-D-allofuranose

There total 1 articles about O³-benzyl-O¹,O²-isopropylidene-O⁵,O⁶-bis-methanesulfonyl-α-D-allofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ O3-benzyl-O1,O2-isopropylidene-O5,O6-bis-methanesulfonyl-α-D-allofuranose (22331-20-0)

Guidance literature:

DOI:10.1016/S0008-6215(00)81693-6

Reference yield: 90.0%

O3-benzyl-O1,O2-isopropylidene-O5,O6-bis-methanesulfonyl-α-D-allofuranose (22331-20-0) → 5,6-dideoxy-3-O-benzyl-1,2-O-isopropylidene-α-D-xylofuranose (23537-43-1)

Guidance literature:

With sodium iodide; In butanone; for 12h; Heating;

DOI:10.1080/07328309808002321

Reference yield:

O3-benzyl-O1,O2-isopropylidene-O5,O6-bis-methanesulfonyl-α-D-allofuranose (22331-20-0) → (2R,3R,4S,5R)-4-Benzyloxy-5-vinyl-tetrahydro-furan-2,3-diol

Guidance literature:

Multi-step reaction with 2 steps

1: 90 percent / NaI / butan-2-one / 12 h / Heating

2: 2 N HCl / tetrahydrofuran / 4 h / Heating

With hydrogenchloride; sodium iodide; In tetrahydrofuran; butanone;

DOI:10.1080/07328309808002321

Downstream raw materials:

O³-benzyl-5,6-diazane-1,1-diyl-O¹,O²-isopropylidene-β-L-5,6-dideoxy-talofuranose

5,6-dideoxy-3-O-benzyl-1,2-O-isopropylidene-α-D-xylofuranose

O³-benzyl-5,6-(2-benzylidene-diazane-1,1-diyl)-O¹,O²-isopropylidene-β-L-5,6-dideoxy-talofuranose

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