(isopropylthio)phenylmethyl <(isopropylthio)phenylmethyl>isopropylphosphinodithioate

Base Information

• Chemical Name: (isopropylthio)phenylmethyl <(isopropylthio)phenylmethyl>isopropylphosphinodithioate
• CAS No.: 135578-55-1
• Molecular Formula: C₂₃H₃₃PS₄
• Molecular Weight: 468.753

Synonyms:(isopropylthio)phenylmethyl <(isopropylthio)phenylmethyl>isopropylphosphinodithioate

Chemical Property of (isopropylthio)phenylmethyl <(isopropylthio)phenylmethyl>isopropylphosphinodithioate

Chemical Property:

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Technology Process of (isopropylthio)phenylmethyl <(isopropylthio)phenylmethyl>isopropylphosphinodithioate

There total 2 articles about (isopropylthio)phenylmethyl <(isopropylthio)phenylmethyl>isopropylphosphinodithioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.1%

1-phenyl-1,1-bis(i-propylthio)methane (135578-61-9) → triisopropyl tetrathiophosphate (2386-41-6) + benzyl(isopropyl)sulfane (770-34-3) + diisopropyl (isopropylthio)phenylmethylphosphonotrithioate (135578-54-0) + (isopropylthio)phenylmethyl <(isopropylthio)phenylmethyl>isopropylphosphinodithioate (135578-55-1)

Guidance literature:

With tetraphosphorus trisulfide; triethylamine; at 130 - 140 ℃; for 12h; other substrates; in presence of other amines;

Reference yield: 16.0%

1-phenyl-1,1-bis(i-propylthio)methane (135578-61-9) → diisopropyl (isopropylthio)phenylmethylphosphonotrithioate (135578-54-0) + (isopropylthio)phenylmethyl <(isopropylthio)phenylmethyl>isopropylphosphinodithioate (135578-55-1)

Guidance literature:

With P₄S₅; In toluene; at 130 - 140 ℃; for 1h;

upstream raw materials:

1-phenyl-1,1-bis(i-propylthio)methane

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