(3,4-di-O-benzyl-6-azido-2-N-(tert-butyloxycarbonyl)amino-2-deoxy-α-D-glucopyranosyl)-(1->6)-2,3,4,5-tetra-O-benzyl-L-myo-inositol

Base Information

Chemical Name:(3,4-di-O-benzyl-6-azido-2-N-(tert-butyloxycarbonyl)amino-2-deoxy-α-D-glucopyranosyl)-(1->6)-2,3,4,5-tetra-O-benzyl-L-myo-inositol
CAS No.:1323371-60-3
Molecular Formula:C₅₉H₆₆N₄O₁₁
Molecular Weight:1007.19
Hs Code.:

Synonyms:(3,4-di-O-benzyl-6-azido-2-N-(tert-butyloxycarbonyl)amino-2-deoxy-α-D-glucopyranosyl)-(1->6)-2,3,4,5-tetra-O-benzyl-L-myo-inositol

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Chemical Property of (3,4-di-O-benzyl-6-azido-2-N-(tert-butyloxycarbonyl)amino-2-deoxy-α-D-glucopyranosyl)-(1->6)-2,3,4,5-tetra-O-benzyl-L-myo-inositol

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Technology Process of (3,4-di-O-benzyl-6-azido-2-N-(tert-butyloxycarbonyl)amino-2-deoxy-α-D-glucopyranosyl)-(1->6)-2,3,4,5-tetra-O-benzyl-L-myo-inositol

There total 4 articles about (3,4-di-O-benzyl-6-azido-2-N-(tert-butyloxycarbonyl)amino-2-deoxy-α-D-glucopyranosyl)-(1->6)-2,3,4,5-tetra-O-benzyl-L-myo-inositol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 1323371-54-5
(3,4-di-O-benzyl-6-azido-2-N-(tert-butyloxycarbonyl)amino-2-deoxy-α-D-glucopyranosyl)-(1->6)-1-O-p-methoxybenzyl-2,3,4,5-tetra-O-benzyl-L-myo-inositol

: 1323371-60-3
(3,4-di-O-benzyl-6-azido-2-N-(tert-butyloxycarbonyl)amino-2-deoxy-α-D-glucopyranosyl)-(1->6)-2,3,4,5-tetra-O-benzyl-L-myo-inositol

Guidance literature:: With water; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; at 0 - 20 ℃; for 3h; Inert atmosphere;
DOI:10.1016/j.tetlet.2011.06.005

Reference yield:

: 1323371-50-1
(3,4-di-O-benzyl-6-O-acetyl-2-N-(tert-butyloxycarbonyl)amino-2-deoxy-α-D-glucopyranosyl)-(1->6)-1-O-p-methoxybenzyl-2,3,4,5-tetra-O-benzyl-L-myo-inositol

: 1323371-60-3
(3,4-di-O-benzyl-6-azido-2-N-(tert-butyloxycarbonyl)amino-2-deoxy-α-D-glucopyranosyl)-(1->6)-2,3,4,5-tetra-O-benzyl-L-myo-inositol

Guidance literature:: Multi-step reaction with 4 steps

1: methanol; sodium methylate / dichloromethane / 2 h / 20 °C / Inert atmosphere

2: pyridine / 3 h / 0 - 20 °C / Inert atmosphere; Molecular sieve

3: sodium azide / N,N-dimethyl-formamide / 3 h / 110 - 120 °C / Inert atmosphere

4: water; 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere

With pyridine; methanol; sodium azide; water; sodium methylate; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.tetlet.2011.06.005

Reference yield:

: C₆₇H₇₅NO₁₃

: 1323371-60-3
(3,4-di-O-benzyl-6-azido-2-N-(tert-butyloxycarbonyl)amino-2-deoxy-α-D-glucopyranosyl)-(1->6)-2,3,4,5-tetra-O-benzyl-L-myo-inositol

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / 3 h / 0 - 20 °C / Inert atmosphere; Molecular sieve

2: sodium azide / N,N-dimethyl-formamide / 3 h / 110 - 120 °C / Inert atmosphere

3: water; 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere

With pyridine; sodium azide; water; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.tetlet.2011.06.005