3-(N-(2-(naphthalen-2-ylamino)-2-oxoethyl)sulfamoyl)benzamidinium trifluoroacetate

Base Information

Chemical Name:3-(N-(2-(naphthalen-2-ylamino)-2-oxoethyl)sulfamoyl)benzamidinium trifluoroacetate
CAS No.:1403957-49-2
Molecular Formula:C₂HF₃O₂*C₁₉H₁₈N₄O₃S
Molecular Weight:496.467
Hs Code.:

Synonyms:3-(N-(2-(naphthalen-2-ylamino)-2-oxoethyl)sulfamoyl)benzamidinium trifluoroacetate

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Chemical Property of 3-(N-(2-(naphthalen-2-ylamino)-2-oxoethyl)sulfamoyl)benzamidinium trifluoroacetate

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Technology Process of 3-(N-(2-(naphthalen-2-ylamino)-2-oxoethyl)sulfamoyl)benzamidinium trifluoroacetate

There total 5 articles about 3-(N-(2-(naphthalen-2-ylamino)-2-oxoethyl)sulfamoyl)benzamidinium trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: C₂₁H₂₀N₄O₅S

: 76-05-1
trifluoroacetic acid

: 1403957-49-2
3-(N-(2-(naphthalen-2-ylamino)-2-oxoethyl)sulfamoyl)benzamidinium trifluoroacetate

Guidance literature:: C₂₁H₂₀N₄O₅S; With 10% Pd/C; hydrogen; In acetic acid; at 20 ℃; for 1h; under 2280.15 Torr;

trifluoroacetic acid;
DOI:10.1016/j.bmc.2012.08.042

Reference yield:

: 95424-85-4
N-Benzyloxycarbonyl-glycin-

: 1403957-49-2
3-(N-(2-(naphthalen-2-ylamino)-2-oxoethyl)sulfamoyl)benzamidinium trifluoroacetate

Guidance literature:: Multi-step reaction with 5 steps

1: 10% Pd/C; hydrogen / ethyl acetate / 2280.15 Torr

2: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 1 h / 20 °C

3: hydroxylamine hydrochloride; N-ethyl-N,N-diisopropylamine / ethanol / 1 h / 87 °C

4: acetonitrile / 1 h / 20 °C

5: 10% Pd/C; hydrogen / acetic acid / 1 h / 20 °C / 2280.15 Torr

With 10% Pd/C; hydroxylamine hydrochloride; hydrogen; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; ethanol; acetic acid; ethyl acetate; acetonitrile;
DOI:10.1016/j.bmc.2012.08.042

Reference yield:

: 716-94-9,22131-74-4
2-amino-N-(naphthalen-2-yl)acetamide

: 1403957-49-2
3-(N-(2-(naphthalen-2-ylamino)-2-oxoethyl)sulfamoyl)benzamidinium trifluoroacetate

Guidance literature:: Multi-step reaction with 4 steps

1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 1 h / 20 °C

2: hydroxylamine hydrochloride; N-ethyl-N,N-diisopropylamine / ethanol / 1 h / 87 °C

3: acetonitrile / 1 h / 20 °C

4: 10% Pd/C; hydrogen / acetic acid / 1 h / 20 °C / 2280.15 Torr

With 10% Pd/C; hydroxylamine hydrochloride; hydrogen; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; ethanol; acetic acid; acetonitrile;
DOI:10.1016/j.bmc.2012.08.042