Technology Process of C26H34O5
There total 5 articles about C26H34O5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine;
In
dichloromethane;
at 0 ℃;
for 1.5h;
Inert atmosphere;
DOI:10.1021/jo400260m
- Guidance literature:
-
Multi-step reaction with 4 steps
1: trifluorormethanesulfonic acid / dichloromethane; cyclohexane / 0.5 h / 20 °C / Inert atmosphere
2: diisobutylaluminium hydride / dichloromethane; hexane / 0.08 h / -78 °C / Inert atmosphere
3: L-(+)-diisopropyl tartrate; titanium(IV) isopropylate; tert.-butylhydroperoxide / dichloromethane; decane / -20 °C / Inert atmosphere; Molecular sieve
4: dimethyl sulfoxide; sulfur trioxide pyridine complex; triethylamine / dichloromethane / 1.5 h / 0 °C / Inert atmosphere
With
titanium(IV) isopropylate; tert.-butylhydroperoxide; L-(+)-diisopropyl tartrate; trifluorormethanesulfonic acid; sulfur trioxide pyridine complex; diisobutylaluminium hydride; dimethyl sulfoxide; triethylamine;
In
decane; hexane; dichloromethane; cyclohexane;
3: |Sharpless Asymmetric Epoxidation / 4: |Parikh-Doering Oxidation;
DOI:10.1021/jo400260m
- Guidance literature:
-
Multi-step reaction with 5 steps
1: water; trimethylaluminum / dichloromethane; hexane / -40 - 0 °C / Inert atmosphere
2: trifluorormethanesulfonic acid / dichloromethane; cyclohexane / 0.5 h / 20 °C / Inert atmosphere
3: diisobutylaluminium hydride / dichloromethane; hexane / 0.08 h / -78 °C / Inert atmosphere
4: L-(+)-diisopropyl tartrate; titanium(IV) isopropylate; tert.-butylhydroperoxide / dichloromethane; decane / -20 °C / Inert atmosphere; Molecular sieve
5: dimethyl sulfoxide; sulfur trioxide pyridine complex; triethylamine / dichloromethane / 1.5 h / 0 °C / Inert atmosphere
With
titanium(IV) isopropylate; tert.-butylhydroperoxide; L-(+)-diisopropyl tartrate; trifluorormethanesulfonic acid; water; trimethylaluminum; sulfur trioxide pyridine complex; diisobutylaluminium hydride; dimethyl sulfoxide; triethylamine;
In
decane; hexane; dichloromethane; cyclohexane;
4: |Sharpless Asymmetric Epoxidation / 5: |Parikh-Doering Oxidation;
DOI:10.1021/jo400260m