N-Benzyl-N-[(S)-1-((S)-2,2-dimethyl-[1,3]dioxolan-4-yl)-prop-2-ynyl]-hydroxylamine

Base Information

Chemical Name:N-Benzyl-N-[(S)-1-((S)-2,2-dimethyl-[1,3]dioxolan-4-yl)-prop-2-ynyl]-hydroxylamine
CAS No.:198418-07-4
Molecular Formula:C₁₅H₁₉NO₃
Molecular Weight:261.321
Hs Code.:

Synonyms:N-Benzyl-N-[(S)-1-((S)-2,2-dimethyl-[1,3]dioxolan-4-yl)-prop-2-ynyl]-hydroxylamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-Benzyl-N-[(S)-1-((S)-2,2-dimethyl-[1,3]dioxolan-4-yl)-prop-2-ynyl]-hydroxylamine

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Technology Process of N-Benzyl-N-[(S)-1-((S)-2,2-dimethyl-[1,3]dioxolan-4-yl)-prop-2-ynyl]-hydroxylamine

There total 4 articles about N-Benzyl-N-[(S)-1-((S)-2,2-dimethyl-[1,3]dioxolan-4-yl)-prop-2-ynyl]-hydroxylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 181303-70-8
N-Benzyl-N-[(S)-1-((S)-2,2-dimethyl-[1,3]dioxolan-4-yl)-3-trimethylsilanyl-prop-2-ynyl]-hydroxylamine

: 198418-07-4
N-Benzyl-N-[(S)-1-((S)-2,2-dimethyl-[1,3]dioxolan-4-yl)-prop-2-ynyl]-hydroxylamine

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; for 0.0333333h; Ambient temperature;
DOI:10.1016/S0957-4166(97)00438-2

Reference yield:

: 91190-38-4,111058-38-9,1165677-00-8
N-benzyl-2,3-O-isopropylidene-D-glyceraldehyde nitrone

: 198418-07-4
N-Benzyl-N-[(S)-1-((S)-2,2-dimethyl-[1,3]dioxolan-4-yl)-prop-2-ynyl]-hydroxylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) Et₂AlCl / 1.) Et₂O, hexane, RT, 5 min, 2.) THF, Et₂O, hexane, -80 deg C, 60 min

2: 90 percent / Bu₄NF / tetrahydrofuran / 0.03 h / Ambient temperature

With tetrabutyl ammonium fluoride; diethylaluminium chloride; In tetrahydrofuran;
DOI:10.1016/S0957-4166(97)00438-2

Reference yield:

: 622-30-0
N-benzyl hydroxylalmine

: 198418-07-4
N-Benzyl-N-[(S)-1-((S)-2,2-dimethyl-[1,3]dioxolan-4-yl)-prop-2-ynyl]-hydroxylamine

Guidance literature:: Multi-step reaction with 3 steps

1: 82 percent / MgSO₄ / CH₂Cl₂ / 4 h / 20 °C

2: 1.) Et₂AlCl / 1.) Et₂O, hexane, RT, 5 min, 2.) THF, Et₂O, hexane, -80 deg C, 60 min

3: 90 percent / Bu₄NF / tetrahydrofuran / 0.03 h / Ambient temperature

With tetrabutyl ammonium fluoride; diethylaluminium chloride; magnesium sulfate; In tetrahydrofuran; dichloromethane;
DOI:10.1016/S0957-4166(97)00438-2