4-<<6-<<(cyclopentyloxy)carbonyl>amino>benzimidazol-1-yl>methyl>-3-methoxybenzoic acid

Base Information

Chemical Name:4-<<6-<<(cyclopentyloxy)carbonyl>amino>benzimidazol-1-yl>methyl>-3-methoxybenzoic acid
CAS No.:107754-56-3
Molecular Formula:C₂₂H₂₃N₃O₅
Molecular Weight:409.442
Hs Code.:

Synonyms:4-<<6-<<(cyclopentyloxy)carbonyl>amino>benzimidazol-1-yl>methyl>-3-methoxybenzoic acid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-<<6-<<(cyclopentyloxy)carbonyl>amino>benzimidazol-1-yl>methyl>-3-methoxybenzoic acid

Chemical Property:

Purity/Quality:

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Hazard Codes:

MSDS Files:: SDS file from LookChem

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Technology Process of 4-<<6-<<(cyclopentyloxy)carbonyl>amino>benzimidazol-1-yl>methyl>-3-methoxybenzoic acid

There total 6 articles about 4-<<6-<<(cyclopentyloxy)carbonyl>amino>benzimidazol-1-yl>methyl>-3-methoxybenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 107754-53-0
methyl 4-<<6-<<(cyclopentyloxy)carbonyl>amino>benzimidazol-1-yl>methyl>-3-methoxybenzoate

: 107754-56-3
4-<<6-<<(cyclopentyloxy)carbonyl>amino>benzimidazol-1-yl>methyl>-3-methoxybenzoic acid

Guidance literature:: With lithium hydroxide; In tetrahydrofuran; methanol; for 4h;
DOI:10.1021/jm00171a043

Reference yield:

: 50715-28-1
cyclopentyl chloroformate

: 107754-56-3
4-<<6-<<(cyclopentyloxy)carbonyl>amino>benzimidazol-1-yl>methyl>-3-methoxybenzoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / 2,6-lutidine / CH₂Cl₂ / 24 h

2: 78 percent / aq. LiOH / tetrahydrofuran; methanol / 4 h

With 2,6-dimethylpyridine; lithium hydroxide; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/jm00171a043

Reference yield:

: 70264-94-7
methyl 4-(bromomethyl)-3-methoxybenzoate

: 107754-56-3
4-<<6-<<(cyclopentyloxy)carbonyl>amino>benzimidazol-1-yl>methyl>-3-methoxybenzoic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 26 percent / K₂CO₃ / butan-2-one / 24 h / Heating

2: 90 percent / SnCl₂*2H₂O / ethanol / 18 h / 80 °C

3: 93 percent / 2,6-lutidine / CH₂Cl₂ / 24 h

4: 78 percent / aq. LiOH / tetrahydrofuran; methanol / 4 h

With 2,6-dimethylpyridine; lithium hydroxide; potassium carbonate; tin(ll) chloride; In tetrahydrofuran; methanol; ethanol; dichloromethane; butanone;
DOI:10.1021/jm00171a043