(2R,3S)-3-benzyloxycarbonylamino-2-hydroxy-4-phenylbutanoyl-(S)-proline methyl ester

Base Information

Chemical Name:(2R,3S)-3-benzyloxycarbonylamino-2-hydroxy-4-phenylbutanoyl-(S)-proline methyl ester
CAS No.:863640-18-0
Molecular Formula:C₂₄H₂₈N₂O₆
Molecular Weight:440.496
Hs Code.:

Synonyms:(2R,3S)-3-benzyloxycarbonylamino-2-hydroxy-4-phenylbutanoyl-(S)-proline methyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2R,3S)-3-benzyloxycarbonylamino-2-hydroxy-4-phenylbutanoyl-(S)-proline methyl ester

Chemical Property:

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Technology Process of (2R,3S)-3-benzyloxycarbonylamino-2-hydroxy-4-phenylbutanoyl-(S)-proline methyl ester

There total 1 articles about (2R,3S)-3-benzyloxycarbonylamino-2-hydroxy-4-phenylbutanoyl-(S)-proline methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 2133-40-6
L-proline methyl ester monohydrochloride

: 62023-60-3,76498-22-1
(2R,3S)-N-(benzyloxycarbonyl)-3-amino-2-hydroxy-4-phenylbutanoic acid

: 863640-18-0
(2R,3S)-3-benzyloxycarbonylamino-2-hydroxy-4-phenylbutanoyl-(S)-proline methyl ester

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In dichloromethane; at 4 - 20 ℃;
DOI:10.1016/j.bmc.2005.05.040

Reference yield: 16.0%

: 863640-18-0
(2R,3S)-3-benzyloxycarbonylamino-2-hydroxy-4-phenylbutanoyl-(S)-proline methyl ester

: (3R,4S,7S)-4-benzyl-3-hydroxy-1,5-diazabicyclo[5.3.0]decane-2,4-dione

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; at 20 ℃;
DOI:10.1016/j.bmc.2005.05.040

Reference yield:

: 863640-18-0
(2R,3S)-3-benzyloxycarbonylamino-2-hydroxy-4-phenylbutanoyl-(S)-proline methyl ester

: (S)-1-((2R,3S)-3-Amino-2-hydroxy-4-phenyl-butyryl)-pyrrolidine-2-carboxylic acid

Guidance literature:: (2R,3S)-3-benzyloxycarbonylamino-2-hydroxy-4-phenylbutanoyl-(S)-proline methyl ester; With hydrogen; palladium on activated charcoal; In methanol; at 20 ℃;

With sodium hydroxide; In 1,4-dioxane; at 20 ℃;
DOI:10.1016/j.bmc.2005.05.040