6-O-(4-(N-methyl-N-phenylamino)benzyl)-1,2:3,4-di-O-isopropylidene-α-D-galactopyranoside

Base Information

• Chemical Name: 6-O-(4-(N-methyl-N-phenylamino)benzyl)-1,2:3,4-di-O-isopropylidene-α-D-galactopyranoside
• CAS No.: 294637-35-7
• Molecular Formula: C₂₆H₃₃NO₆
• Molecular Weight: 455.551

Synonyms:6-O-(4-(N-methyl-N-phenylamino)benzyl)-1,2:3,4-di-O-isopropylidene-α-D-galactopyranoside

Chemical Property of 6-O-(4-(N-methyl-N-phenylamino)benzyl)-1,2:3,4-di-O-isopropylidene-α-D-galactopyranoside

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Technology Process of 6-O-(4-(N-methyl-N-phenylamino)benzyl)-1,2:3,4-di-O-isopropylidene-α-D-galactopyranoside

There total 7 articles about 6-O-(4-(N-methyl-N-phenylamino)benzyl)-1,2:3,4-di-O-isopropylidene-α-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

N-methylaniline (100-61-8) + 6-O-(4-bromobenzyl)-1,2:3,4-di-O-isopropylidene-α-D-galactopyranoside (294637-29-9) → 6-O-(4-(N-methyl-N-phenylamino)benzyl)-1,2:3,4-di-O-isopropylidene-α-D-galactopyranoside (294637-35-7)

Guidance literature:

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; johnphos; sodium t-butanolate; In toluene; at 80 ℃; for 5h;

DOI:10.1021/ja0008665

Reference yield: 96.0%

N-methylaniline (100-61-8) + 6-O-(4-iodobenzyl)-1,2:3,4-di-O-isopropylidene-α-D-galactopyranoside → 6-O-(4-(N-methyl-N-phenylamino)benzyl)-1,2:3,4-di-O-isopropylidene-α-D-galactopyranoside (294637-35-7)

Guidance literature:

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 1-(N,N-dimethylamino)-1'-(dicyclohexylphosphino)biphenyl; sodium t-butanolate; In toluene; at 20 ℃;

DOI:10.1021/ja0008665

Reference yield: 89.0%

N-methylaniline (100-61-8) + 6-O-(4-chlorobenzyl)-1,2:3,4-di-O-isopropylidene-α-D-galactopyranoside (294637-30-2) → 6-O-(4-(N-methyl-N-phenylamino)benzyl)-1,2:3,4-di-O-isopropylidene-α-D-galactopyranoside (294637-35-7)

Guidance literature:

With palladium diacetate; johnphos; sodium t-butanolate; In toluene; at 20 ℃;

DOI:10.1021/ja0008665

upstream raw materials:

N-methylaniline

6-O-(4-bromobenzyl)-1,2:3,4-di-O-isopropylidene-α-D-galactopyranoside

6-O-(4-chlorobenzyl)-1,2:3,4-di-O-isopropylidene-α-D-galactopyranoside

1-bromomethyl-4-iodobenzene

Downstream raw materials:

1,2:3,4-di-O-isopropylidene-α-D-galactopyranose

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