2,6-dimethyl-3,4-dihydro-2H-1,4-benzoxazin-3-one

Base Information

Chemical Name:2,6-dimethyl-3,4-dihydro-2H-1,4-benzoxazin-3-one
CAS No.:17959-90-9
Molecular Formula:C₁₀H₁₁NO₂
Molecular Weight:177.203
Hs Code.:2934999090
DSSTox Substance ID:DTXSID20398810
Nikkaji Number:J2.816.749K
Mol file:17959-90-9.mol

Synonyms:17959-90-9;2,6-dimethyl-3,4-dihydro-2H-1,4-benzoxazin-3-one;2,6-dimethyl-4H-1,4-benzoxazin-3-one;2,6-DIMETHYL-2H-BENZO[B][1,4]OXAZIN-3(4H)-ONE;2,6-DIMETHYL-2,4-DIHYDRO-1,4-BENZOXAZIN-3-ONE;2,6-Dimethyl-4H-benzo[1,4]oxazin-3-one;2,6-dimethyl-2H-1,4-benzoxazin-3(4H)-one;SCHEMBL5670717;DTXSID20398810;AUNQUXZPFSCXMN-UHFFFAOYSA-N;MFCD01833988;STL364650;2,6-Dimethyl-1,4-benzoxazin-3-one;AKOS000421489;AKOS016352762;CS-0207132;EU-0063329;EN300-98567;2,6-Dimethyl-2H-1,4-benzooxazine-3(4H)-one;Z274567878

Suppliers and Price of 2,6-dimethyl-3,4-dihydro-2H-1,4-benzoxazin-3-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
2,6-dimethyl-3,4-dihydro-2H-1,4-benzoxazin-3-one
500mg
$ 285.00

TRC
2,6-dimethyl-3,4-dihydro-2H-1,4-benzoxazin-3-one
100mg
$ 65.00

SynQuest Laboratories
2,6-Dimethyl-2H-1,4-benzoxazin-3(4H)-one
1 g
$ 199.00

Matrix Scientific
2-Chloro-N-(2-hydroxy-5-methylphenyl)propanamide
1g
$ 300.00

Matrix Scientific
2,6-Dimethyl-2H-1,4-benzoxazin-3(4H)-one
1g
$ 240.00

Heterocyclics
2,6-Dimethyl-2H-benzo[b][1,4]oxazin-3(4H)-one 97%
1g
$ 175.00

Heterocyclics
2,6-Dimethyl-2H-benzo[b][1,4]oxazin-3(4H)-one 97%
5g
$ 550.00

Crysdot
2,6-Dimethyl-2H-benzo[b][1,4]oxazin-3(4H)-one 95+%
5g
$ 508.00

Crysdot
2,6-Dimethyl-2H-benzo[b][1,4]oxazin-3(4H)-one 95+%
10g
$ 771.00

American Custom Chemicals Corporation
2,6-DIMETHYL-2H-BENZO[B][1,4]OXAZIN-3(4H)-ONE 95.00%
5G
$ 1590.46

Total 5 raw suppliers

Chemical Property of 2,6-dimethyl-3,4-dihydro-2H-1,4-benzoxazin-3-one

Chemical Property:

PSA：41.82000
LogP:1.79950
XLogP3:1.6
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:0
Exact Mass:177.078978594
Heavy Atom Count:13
Complexity:217

Purity/Quality:

97% ^*data from raw suppliers

2,6-dimethyl-3,4-dihydro-2H-1,4-benzoxazin-3-one ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1C(=O)NC2=C(O1)C=CC(=C2)C

Technology Process of 2,6-dimethyl-3,4-dihydro-2H-1,4-benzoxazin-3-one

There total 5 articles about 2,6-dimethyl-3,4-dihydro-2H-1,4-benzoxazin-3-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1248141-64-1
2-(4-methyl-2-nitrophenoxy)propanenitrile

: 17959-90-9
3,4-dihydro-2,6-dimethyl-3-oxo-2H-1,4-benzoxazine

Guidance literature:: With iron; acetic acid; for 2.5h; Inert atmosphere; Reflux;
DOI:10.1016/j.tet.2010.11.095

Reference yield: 88.0%

: 95-84-1
3-amino-4-hydroxytoluene

: 535-11-5,41978-69-2
Ethyl 2-bromopropionate

: 17959-90-9
3,4-dihydro-2,6-dimethyl-3-oxo-2H-1,4-benzoxazine

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; 1-octyl-3-methylimidazolium tetrafluoroborate; at 20 ℃; for 0.5h; chemoselective reaction;
DOI:10.1016/j.tetlet.2010.01.122