4-methoxyphenyl(benzylamine)phosphonodithioate benzylamine salt

Base Information

• Chemical Name: 4-methoxyphenyl(benzylamine)phosphonodithioate benzylamine salt
• CAS No.: 78906-56-6
• Molecular Formula: C₇H₉N*C₁₄H₁₆NOPS₂
• Molecular Weight: 416.548
• Mol file: 78906-56-6.mol

Synonyms:4-methoxyphenyl(benzylamine)phosphonodithioate benzylamine salt

Chemical Property of 4-methoxyphenyl(benzylamine)phosphonodithioate benzylamine salt

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of 4-methoxyphenyl(benzylamine)phosphonodithioate benzylamine salt

There total 1 articles about 4-methoxyphenyl(benzylamine)phosphonodithioate benzylamine salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

Lawessons reagent (19172-47-5,94367-93-8) + benzylamine (100-46-9) → 4-methoxyphenyl(benzylamine)phosphonodithioate benzylamine salt (78906-56-6)

Guidance literature:

In toluene; at 20 ℃; for 6h;

DOI:10.1016/j.poly.2016.09.002

Reference yield: 88.0%

4-methoxyphenyl(benzylamine)phosphonodithioate benzylamine salt (78906-56-6) + palladium dichloride → C28H30N2O2P2PdS4

Guidance literature:

In methanol; acetonitrile; for 8h;

DOI:10.1016/j.poly.2016.09.002

Reference yield: 87.0%

4-methoxyphenyl(benzylamine)phosphonodithioate benzylamine salt (78906-56-6) → N,N'-dibenzyl-4-methoxyphenylphosphonothioic diamide (78906-66-8)

Guidance literature:

In xylene; at 140 ℃; for 10h;

DOI:10.1016/S0040-4020(01)97679-3

upstream raw materials:

Lawessons reagent

benzylamine

Downstream raw materials:

S-benzyl N-benzyl-4-methoxyphenylphosphonamidodithioate

N,N'-dibenzyl-4-methoxyphenylphosphonothioic diamide