(2R,3S,6RS)-4-methylbenzenesulfonic acid 6-[pent-4-enyloxy]-3-methyl-2-hydroxyhept-4-ynyl ester

Base Information

Chemical Name:(2R,3S,6RS)-4-methylbenzenesulfonic acid 6-[pent-4-enyloxy]-3-methyl-2-hydroxyhept-4-ynyl ester
CAS No.:370858-92-7
Molecular Formula:C₂₀H₂₈O₅S
Molecular Weight:380.505
Hs Code.:

Synonyms:(2R,3S,6RS)-4-methylbenzenesulfonic acid 6-[pent-4-enyloxy]-3-methyl-2-hydroxyhept-4-ynyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2R,3S,6RS)-4-methylbenzenesulfonic acid 6-[pent-4-enyloxy]-3-methyl-2-hydroxyhept-4-ynyl ester

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Technology Process of (2R,3S,6RS)-4-methylbenzenesulfonic acid 6-[pent-4-enyloxy]-3-methyl-2-hydroxyhept-4-ynyl ester

There total 1 articles about (2R,3S,6RS)-4-methylbenzenesulfonic acid 6-[pent-4-enyloxy]-3-methyl-2-hydroxyhept-4-ynyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 141783-42-8
(2S,3S)-2-(4-methylbenzenesulfonyloxymethyl)-3-methyloxirane

: 154840-34-3
3-(pent-4-enyloxy)-but-1-yne

: 370858-92-7
(2R,3S,6RS)-4-methylbenzenesulfonic acid 6-[pent-4-enyloxy]-3-methyl-2-hydroxyhept-4-ynyl ester

Guidance literature:: 3-(pent-4-enyloxy)-but-1-yne; With n-butyllithium; In diethyl ether; hexane; at -78 ℃; for 0.25h;

With trimethylaluminum; In diethyl ether; hexane; toluene; at -40 ℃; for 1h;

(2S,3S)-2-(4-methylbenzenesulfonyloxymethyl)-3-methyloxirane; With boron trifluoride diethyl etherate; In diethyl ether; hexane; toluene; at -78 ℃; for 4h;
DOI:10.1016/S0040-4020(01)00602-0