N²,N⁴-diisopentyl-6-(1-((4,5-diphenyloxazol-2-yl)methyl)-1H-1,2,3-triazol-4-yl)-1,3,5-triazine-2,4-diamine

Base Information

• Chemical Name: N²,N⁴-diisopentyl-6-(1-((4,5-diphenyloxazol-2-yl)methyl)-1H-1,2,3-triazol-4-yl)-1,3,5-triazine-2,4-diamine
• CAS No.: 1421369-19-8
• Molecular Formula: C₃₁H₃₇N₉O
• Molecular Weight: 551.694

Synonyms:N²,N⁴-diisopentyl-6-(1-((4,5-diphenyloxazol-2-yl)methyl)-1H-1,2,3-triazol-4-yl)-1,3,5-triazine-2,4-diamine

Chemical Property of N²,N⁴-diisopentyl-6-(1-((4,5-diphenyloxazol-2-yl)methyl)-1H-1,2,3-triazol-4-yl)-1,3,5-triazine-2,4-diamine

Chemical Property:

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Technology Process of N²,N⁴-diisopentyl-6-(1-((4,5-diphenyloxazol-2-yl)methyl)-1H-1,2,3-triazol-4-yl)-1,3,5-triazine-2,4-diamine

There total 4 articles about N²,N⁴-diisopentyl-6-(1-((4,5-diphenyloxazol-2-yl)methyl)-1H-1,2,3-triazol-4-yl)-1,3,5-triazine-2,4-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

2-(azidomethyl)-4,5-diphenyloxazole (1401734-75-5) + 6-ethynyl-N2,N4-diisopentyl-1,3,5-triazine-2,4-diamine → N2,N4-diisopentyl-6-(1-((4,5-diphenyloxazol-2-yl)methyl)-1H-1,2,3-triazol-4-yl)-1,3,5-triazine-2,4-diamine (1421369-19-8)

Guidance literature:

With copper(ll) sulfate pentahydrate; sodium L-ascorbate; In tetrahydrofuran; water; at 20 ℃; for 16h;

DOI:10.1016/j.bmc.2016.08.059

Reference yield:

2-(chloromethyl)-4,5-diphenyloxazole (33161-99-8) → N2,N4-diisopentyl-6-(1-((4,5-diphenyloxazol-2-yl)methyl)-1H-1,2,3-triazol-4-yl)-1,3,5-triazine-2,4-diamine (1421369-19-8)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium azide / N,N-dimethyl-formamide / 3 h / 20 °C / Inert atmosphere

2: copper(ll) sulfate pentahydrate; sodium L-ascorbate / tetrahydrofuran; water / 16 h / 20 °C

With sodium azide; copper(ll) sulfate pentahydrate; sodium L-ascorbate; In tetrahydrofuran; water; N,N-dimethyl-formamide;

DOI:10.1016/j.bmc.2016.08.059

Reference yield:

2-hydroxy-2-phenylacetophenone (119-53-9,579-44-2) → N2,N4-diisopentyl-6-(1-((4,5-diphenyloxazol-2-yl)methyl)-1H-1,2,3-triazol-4-yl)-1,3,5-triazine-2,4-diamine (1421369-19-8)

Guidance literature:

Multi-step reaction with 4 steps

1: dmap / dichloromethane / 16 h / 0 - 20 °C / Inert atmosphere

2: ammonium acetate; acetic acid / 3 h / 115 °C / Inert atmosphere

3: sodium azide / N,N-dimethyl-formamide / 3 h / 20 °C / Inert atmosphere

4: copper(ll) sulfate pentahydrate; sodium L-ascorbate / tetrahydrofuran; water / 16 h / 20 °C

With dmap; sodium azide; copper(ll) sulfate pentahydrate; ammonium acetate; acetic acid; sodium L-ascorbate; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide;

DOI:10.1016/j.bmc.2016.08.059

upstream raw materials:

2-(chloromethyl)-4,5-diphenyloxazole

2-(azidomethyl)-4,5-diphenyloxazole

2-hydroxy-2-phenylacetophenone

2-oxo-1,2-diphenylethyl-2-chloroacetate

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