2-Methoxy-dibenzosuberone

Base Information

Chemical Name:2-Methoxy-dibenzosuberone
CAS No.:17910-72-4
Molecular Formula:C16H14 O2
Molecular Weight:238.286
Hs Code.:2914509090
DSSTox Substance ID:DTXSID801201776
Nikkaji Number:J966.550A
Mol file:17910-72-4.mol

Synonyms:2-METHOXY-DIBENZOSUBERONE;17910-72-4;2-Methoxy-10,11-dihydro-5H-dibenzo[a,d][7]annulen-5-one;6-methoxytricyclo[9.4.0.03,8]pentadeca-1(15),3(8),4,6,11,13-hexaen-2-one;2-methoxydibenzosuberone;SCHEMBL3759572;BRFQZKLQUBMUAM-UHFFFAOYSA-N;DTXSID801201776;MFCD04114365;AKOS005216069;AB18157;CS-0336766;2-Methoxy-11H-dibenzo[a,d]cycloheptene-5(10H)-one;2-methoxy-10,11-dihydro-dibenzo[a,d]cyclohepten-5-one;2-Methoxy-10,11-dihydro-5H-dibenzo[a,d]cyclohepten-5-one

Suppliers and Price of 2-Methoxy-dibenzosuberone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

J&W Pharmlab
2-Methoxy-dibenzosuberone 98%
100mg
$ 212.00

J&W Pharmlab
2-Methoxy-dibenzosuberone 98%
1g
$ 998.00

Crysdot
2-Methoxy-10,11-dihydro-5H-dibenzo[a,d][7]annulen-5-one 95+%
1g
$ 672.00

American Custom Chemicals Corporation
2-METHOXY-DIBENZOSUBERONE 98.00%
5MG
$ 505.11

Alichem
2-Methoxy-10,11-dihydro-5H-dibenzo[a,d][7]annulen-5-one
1g
$ 574.35

Total 8 raw suppliers

Chemical Property of 2-Methoxy-dibenzosuberone

Chemical Property:

Boiling Point:418.2±45.0 °C(Predicted)
PSA：26.30000
Density:1.166±0.06 g/cm3(Predicted)
LogP:3.02480
XLogP3:3.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:238.099379685
Heavy Atom Count:18
Complexity:312

Purity/Quality:

97% ^*data from raw suppliers

2-Methoxy-dibenzosuberone 98% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC2=C(C=C1)C(=O)C3=CC=CC=C3CC2

Technology Process of 2-Methoxy-dibenzosuberone

There total 14 articles about 2-Methoxy-dibenzosuberone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 17910-71-3
2-<2-(3-methoxyphenyl)ethyl>benzoic acid

: 17910-72-4
2-methoxy-10,11-dihydro-5H-dibenzo[a,d]cyclohepten-5-one

Guidance literature:: With PPA; at 145 - 150 ℃; for 0.833333h;
DOI:10.1021/jo00105a010

Reference yield: 55.0%

: 14525-71-4
2-<3-(4-methoxyphenyl)ethyl>benzoic acid

: 17910-72-4
2-methoxy-10,11-dihydro-5H-dibenzo[a,d]cyclohepten-5-one

Guidance literature:: With phosphorus pentoxide; In xylene; Heating;
DOI:10.1021/jm00091a017

Reference yield:

: 85-44-9
phthalic anhydride

: 17910-72-4
2-methoxy-10,11-dihydro-5H-dibenzo[a,d]cyclohepten-5-one

Guidance literature:: Multi-step reaction with 3 steps

1: 77 percent / CH₃COONa / 6 h / 230 - 245 °C

2: 81 percent / H₂, TEA / W-2 Raney Ni / tetrahydrofuran / 30 h / 50 °C / 2942.03 Torr

3: 86 percent / PPA / 0.83 h / 145 - 150 °C

With TEA; hydrogen; sodium acetate; W-2 Raney Ni; In tetrahydrofuran;
DOI:10.1021/jo00105a010