Technology Process of C25H40ClN3O3Si
There total 8 articles about C25H40ClN3O3Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 39 percent / CuI; tert-butylnitrite / acetonitrile / 3 h / 65 °C
2: Cs2CO3 / Pd2(dba)3; chiral ferrocenyl catalyst / toluene; dimethylsulfoxide / 48 h / 100 °C
With
copper(l) iodide; tert.-butylnitrite; caesium carbonate;
tris(dibenzylideneacetone)dipalladium (0); chiral ferrocenyl catalyst;
In
dimethyl sulfoxide; toluene; acetonitrile;
DOI:10.1021/jm070312d
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 95 percent / conc. HCl; EtOH / 0.5 h / Heating
2: 39 percent / CuI; tert-butylnitrite / acetonitrile / 3 h / 65 °C
3: Cs2CO3 / Pd2(dba)3; chiral ferrocenyl catalyst / toluene; dimethylsulfoxide / 48 h / 100 °C
With
hydrogenchloride; copper(l) iodide; tert.-butylnitrite; ethanol; caesium carbonate;
tris(dibenzylideneacetone)dipalladium (0); chiral ferrocenyl catalyst;
In
dimethyl sulfoxide; toluene; acetonitrile;
DOI:10.1021/jm070312d
- Guidance literature:
-
Multi-step reaction with 3 steps
1: NaN3 / dimethylformamide / 80 °C
2: H2 / Pd/C / methanol / 3 h
3: Cs2CO3 / Pd2(dba)3; chiral ferrocenyl catalyst / toluene; dimethylsulfoxide / 48 h / 100 °C
With
sodium azide; hydrogen; caesium carbonate;
palladium on activated charcoal; tris(dibenzylideneacetone)dipalladium (0); chiral ferrocenyl catalyst;
In
methanol; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene;
DOI:10.1021/jm070312d
