(S)-2-[(3S,4R)-2-Oxo-3-((S)-2-oxo-4-phenyl-oxazolidin-3-yl)-4-phenyl-azetidin-1-yl]-succinic acid 1-tert-butyl ester 4-ethyl ester

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Chemical Name:(S)-2-[(3S,4R)-2-Oxo-3-((S)-2-oxo-4-phenyl-oxazolidin-3-yl)-4-phenyl-azetidin-1-yl]-succinic acid 1-tert-butyl ester 4-ethyl ester
CAS No.:123932-18-3
Molecular Formula:C₂₈H₃₂N₂O₇
Molecular Weight:508.571
Hs Code.:

Synonyms:(S)-2-[(3S,4R)-2-Oxo-3-((S)-2-oxo-4-phenyl-oxazolidin-3-yl)-4-phenyl-azetidin-1-yl]-succinic acid 1-tert-butyl ester 4-ethyl ester

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Chemical Property of (S)-2-[(3S,4R)-2-Oxo-3-((S)-2-oxo-4-phenyl-oxazolidin-3-yl)-4-phenyl-azetidin-1-yl]-succinic acid 1-tert-butyl ester 4-ethyl ester

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Technology Process of (S)-2-[(3S,4R)-2-Oxo-3-((S)-2-oxo-4-phenyl-oxazolidin-3-yl)-4-phenyl-azetidin-1-yl]-succinic acid 1-tert-butyl ester 4-ethyl ester

There total 7 articles about (S)-2-[(3S,4R)-2-Oxo-3-((S)-2-oxo-4-phenyl-oxazolidin-3-yl)-4-phenyl-azetidin-1-yl]-succinic acid 1-tert-butyl ester 4-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6456-74-2
Glycine tert-butyl ester

: 123932-18-3
(S)-2-[(3S,4R)-2-Oxo-3-((S)-2-oxo-4-phenyl-oxazolidin-3-yl)-4-phenyl-azetidin-1-yl]-succinic acid 1-tert-butyl ester 4-ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / sodium sulfate / benzene / Ambient temperature

2: 83 percent / CH₂Cl₂ / -78 deg C to RT

3: 1.) LHMDS / 1.) THF, hexane, -78 deg C, 2.) -30 deg C

With sodium sulfate; lithium hexamethyldisilazane; In dichloromethane; benzene;
DOI:10.1021/ja00158a041

Reference yield:

: 64923-12-2
tert-butyl N-benzylideneglycinate

: 123932-18-3
(S)-2-[(3S,4R)-2-Oxo-3-((S)-2-oxo-4-phenyl-oxazolidin-3-yl)-4-phenyl-azetidin-1-yl]-succinic acid 1-tert-butyl ester 4-ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / CH₂Cl₂ / -78 deg C to RT

2: 1.) LHMDS / 1.) THF, hexane, -78 deg C, 2.) -30 deg C

With lithium hexamethyldisilazane; In dichloromethane;
DOI:10.1021/ja00158a041

Reference yield:

: 108493-67-0
(S)-(4-phenyloxazolidinyl)ketene

: 123932-18-3
(S)-2-[(3S,4R)-2-Oxo-3-((S)-2-oxo-4-phenyl-oxazolidin-3-yl)-4-phenyl-azetidin-1-yl]-succinic acid 1-tert-butyl ester 4-ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / CH₂Cl₂ / -78 deg C to RT

2: 1.) LHMDS / 1.) THF, hexane, -78 deg C, 2.) -30 deg C

With lithium hexamethyldisilazane; In dichloromethane;
DOI:10.1021/ja00158a041