Technology Process of C32H37N5O3Si
There total 10 articles about C32H37N5O3Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium cyanide;
In
ethanol; water;
at 80 ℃;
for 48h;
Sealed tube;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: potassium hydroxide; water / ethanol / 2 h / Reflux
1.2: 16 h
2.1: N-ethyl-N,N-diisopropylamine; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide / N,N-dimethyl-formamide / 0.25 h / 0 °C
2.2: 15 h / 0 °C
2.3: 16 h / 0 - 20 °C
3.1: tetrahydrofuran / 2 h / -78 °C
4.1: potassium carbonate / tetrahydrofuran; water / 0.5 h / 20 °C / Inert atmosphere
4.2: 12 h / 80 °C
5.1: potassium cyanide / ethanol; water / 48 h / 80 °C / Sealed tube
With
potassium cyanide; water; potassium carbonate; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; N-ethyl-N,N-diisopropylamine; potassium hydroxide;
In
tetrahydrofuran; ethanol; water; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: N-ethyl-N,N-diisopropylamine; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide / N,N-dimethyl-formamide / 0.25 h / 0 °C
1.2: 15 h / 0 °C
1.3: 16 h / 0 - 20 °C
2.1: tetrahydrofuran / 2 h / -78 °C
3.1: potassium carbonate / tetrahydrofuran; water / 0.5 h / 20 °C / Inert atmosphere
3.2: 12 h / 80 °C
4.1: potassium cyanide / ethanol; water / 48 h / 80 °C / Sealed tube
With
potassium cyanide; potassium carbonate; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; ethanol; water; N,N-dimethyl-formamide;
