6-(2,4,6-trioxo-5-phenylhexahydropyrimidin-5-yl)hexyl 4-methylbenzenesulfonate

Base Information

Chemical Name:6-(2,4,6-trioxo-5-phenylhexahydropyrimidin-5-yl)hexyl 4-methylbenzenesulfonate
CAS No.:1416792-29-4
Molecular Formula:C₂₃H₂₆N₂O₆S
Molecular Weight:458.535
Hs Code.:

Synonyms:6-(2,4,6-trioxo-5-phenylhexahydropyrimidin-5-yl)hexyl 4-methylbenzenesulfonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6-(2,4,6-trioxo-5-phenylhexahydropyrimidin-5-yl)hexyl 4-methylbenzenesulfonate

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Technology Process of 6-(2,4,6-trioxo-5-phenylhexahydropyrimidin-5-yl)hexyl 4-methylbenzenesulfonate

There total 4 articles about 6-(2,4,6-trioxo-5-phenylhexahydropyrimidin-5-yl)hexyl 4-methylbenzenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 297175-04-3
5-(6-hydroxyhexyl)-5-phenylpyrimidine-2,4,6(1H,3H,5H)-trione

: 98-59-9
p-toluenesulfonyl chloride

: 1416792-29-4
6-(2,4,6-trioxo-5-phenylhexahydropyrimidin-5-yl)hexyl 4-methylbenzenesulfonate

Guidance literature:: With pyridine; In chloroform; at 0 - 60 ℃; Inert atmosphere;
DOI:10.1039/c2cc38443d

Reference yield: 65.0%

: 1416792-29-4
6-(2,4,6-trioxo-5-phenylhexahydropyrimidin-5-yl)hexyl 4-methylbenzenesulfonate

Guidance literature:: With pyridine; In chloroform; at 20 ℃; for 96h; Cooling with ice; Inert atmosphere;

Reference yield:

: 54247-27-7
1-bromo-6-benzyloxyhexane

: 1416792-29-4
6-(2,4,6-trioxo-5-phenylhexahydropyrimidin-5-yl)hexyl 4-methylbenzenesulfonate

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 0 °C / Inert atmosphere

1.2: 48 h / 20 °C / Inert atmosphere

2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 2 h / 0 °C / Inert atmosphere

2.2: 2.5 h / 20 °C / Inert atmosphere

3.1: hydrogen; 20% palladium hydroxide on charcoal / methanol / 15 h / 20 °C

4.1: pyridine / chloroform / 0 - 60 °C / Inert atmosphere

With pyridine; 20% palladium hydroxide on charcoal; hydrogen; sodium hydride; In methanol; chloroform; N,N-dimethyl-formamide; mineral oil;
DOI:10.1039/c2cc38443d