Technology Process of C26H27NO4
There total 5 articles about C26H27NO4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C16H16BrNO3;
With
tetrakis(triphenylphosphine) palladium(0);
In
benzene;
at 20 ℃;
for 0.666667h;
Inert atmosphere;
5-allyl-2-methoxyphenylboronic acid;
With
potassium carbonate;
In
water; benzene;
for 16h;
Inert atmosphere;
Reflux;
DOI:10.1016/j.bmcl.2011.12.015
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: Jones reagent / acetone / 0.5 h / 0 °C / Inert atmosphere
2.1: zinc dibromide / toluene / 24 h / Reflux; Inert atmosphere; Molecular sieve
3.1: tetrakis(triphenylphosphine) palladium(0) / benzene / 0.67 h / 20 °C / Inert atmosphere
3.2: 16 h / Inert atmosphere; Reflux
With
Jones reagent; tetrakis(triphenylphosphine) palladium(0); zinc dibromide;
In
acetone; toluene; benzene;
2.1: Bohlmann-Rahtz reaction / 3.2: Suzuki-Miyaura coupling;
DOI:10.1016/j.bmcl.2011.12.015
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: zinc dibromide / toluene / 24 h / Reflux; Inert atmosphere; Molecular sieve
2.1: tetrakis(triphenylphosphine) palladium(0) / benzene / 0.67 h / 20 °C / Inert atmosphere
2.2: 16 h / Inert atmosphere; Reflux
With
tetrakis(triphenylphosphine) palladium(0); zinc dibromide;
In
toluene; benzene;
1.1: Bohlmann-Rahtz reaction / 2.2: Suzuki-Miyaura coupling;
DOI:10.1016/j.bmcl.2011.12.015
