(3S,4S)-3-methyl-4-O-β-D-glucopyranosyloctanoic acid

Base Information

Chemical Name:(3S,4S)-3-methyl-4-O-β-D-glucopyranosyloctanoic acid
CAS No.:173355-98-1
Molecular Formula:C₁₅H₂₈O₈
Molecular Weight:336.383
Hs Code.:

Synonyms:(3S,4S)-3-methyl-4-O-β-D-glucopyranosyloctanoic acid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3S,4S)-3-methyl-4-O-β-D-glucopyranosyloctanoic acid

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Technology Process of (3S,4S)-3-methyl-4-O-β-D-glucopyranosyloctanoic acid

There total 1 articles about (3S,4S)-3-methyl-4-O-β-D-glucopyranosyloctanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 89163-43-9,39212-23-2,39638-67-0,55013-32-6,80041-00-5,80041-01-6,99530-35-5,105015-53-0,105119-22-0
cis-5-n-butyl-4-methyl-4,5-dihydro-2(3H)-furanone

: 173355-98-1
(3S,4S)-3-methyl-4-O-β-D-glucopyranosyloctanoic acid

Guidance literature:: Multi-step reaction with 4 steps

1.1: KOH / methanol / 16 h / 20 °C

2.1: 1.59 g / dimethylformamide / 16 h / 20 °C

3.1: AgOTf; 2,6-lutidine / CH₂Cl₂ / 16 h / 20 °C

4.1: NaOMe / methanol / 16 h / 20 °C

4.2: 56 percent / aq. KOH / 16 h / 20 °C

With 2,6-dimethylpyridine; potassium hydroxide; sodium methylate; silver trifluoromethanesulfonate; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2004.05.070