N[(1-benzoyl-4-vinyl-2,3-dihydro-1H-indol-3-yl)acetyl]-2-(ethylsulfinyl)-N-methylacetamide

Base Information

• Chemical Name: N[(1-benzoyl-4-vinyl-2,3-dihydro-1H-indol-3-yl)acetyl]-2-(ethylsulfinyl)-N-methylacetamide
• CAS No.: 269405-60-9
• Molecular Formula: C₂₄H₂₆N₂O₄S
• Molecular Weight: 438.547

Synonyms:N[(1-benzoyl-4-vinyl-2,3-dihydro-1H-indol-3-yl)acetyl]-2-(ethylsulfinyl)-N-methylacetamide

Chemical Property of N[(1-benzoyl-4-vinyl-2,3-dihydro-1H-indol-3-yl)acetyl]-2-(ethylsulfinyl)-N-methylacetamide

Chemical Property:

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Technology Process of N[(1-benzoyl-4-vinyl-2,3-dihydro-1H-indol-3-yl)acetyl]-2-(ethylsulfinyl)-N-methylacetamide

There total 2 articles about N[(1-benzoyl-4-vinyl-2,3-dihydro-1H-indol-3-yl)acetyl]-2-(ethylsulfinyl)-N-methylacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

N[(1-benzoyl-4-vinyl-2,3-dihydro-1H-indol-3-yl)acetyl]-2-(ethylsulfenyl)-N-methylacetamide → N[(1-benzoyl-4-vinyl-2,3-dihydro-1H-indol-3-yl)acetyl]-2-(ethylsulfinyl)-N-methylacetamide (269405-60-9)

Guidance literature:

With sodium periodate; In methanol; water; for 3h;

DOI:10.1021/jo9915729

Reference yield:

2-(1-Benzoyl-4-vinyl-2,3-dihydro-1H-indol-3-yl)-N-methylacetamide (163810-66-0) → N[(1-benzoyl-4-vinyl-2,3-dihydro-1H-indol-3-yl)acetyl]-2-(ethylsulfinyl)-N-methylacetamide (269405-60-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 98 percent / benzene / 12 h / Heating

2: 96 percent / NaIO₄ / methanol; H₂O / 3 h

With sodium periodate; In methanol; water; benzene; 1: Acylation / 2: Oxidation;

DOI:10.1021/jo9915729

Reference yield: 64.0%

acetic anhydride (108-24-7) + N[(1-benzoyl-4-vinyl-2,3-dihydro-1H-indol-3-yl)acetyl]-2-(ethylsulfinyl)-N-methylacetamide (269405-60-9) → 4-benzoyl-9-(ethylsulfenyl)-7-methyl-4,5,5a,7-tetrahydro-6H-indolo[4,3-fg]quinolin-8-one + acetic acid 4-benzoyl-7-methyl-8-oxo-4,5,5a,6,7,8-hexahydroindolo[4,3-fg]quinolin-9-yl ester (269405-61-0)

Guidance literature:

With toluene-4-sulfonic acid; In xylene; for 3h; Heating;

DOI:10.1021/jo9915729

upstream raw materials:

2-(1-Benzoyl-4-vinyl-2,3-dihydro-1H-indol-3-yl)-N-methylacetamide

Downstream raw materials:

acetic acid 4-benzoyl-7-methyl-8-oxo-4,5,5a,6,7,8-hexahydroindolo[4,3-fg]quinolin-9-yl ester

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