(S)-1-((3aS,4S,6S,6aR)-2,2,6-Trimethyl-5-nonyl-tetrahydro-[1,3]dioxolo[4,5-c]pyrrol-4-yl)-2-trityloxy-ethanol

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Chemical Name:(S)-1-((3aS,4S,6S,6aR)-2,2,6-Trimethyl-5-nonyl-tetrahydro-[1,3]dioxolo[4,5-c]pyrrol-4-yl)-2-trityloxy-ethanol
CAS No.:934347-01-0
Molecular Formula:C₃₈H₅₁NO₄
Molecular Weight:585.827
Hs Code.:

Synonyms:(S)-1-((3aS,4S,6S,6aR)-2,2,6-Trimethyl-5-nonyl-tetrahydro-[1,3]dioxolo[4,5-c]pyrrol-4-yl)-2-trityloxy-ethanol

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Chemical Property of (S)-1-((3aS,4S,6S,6aR)-2,2,6-Trimethyl-5-nonyl-tetrahydro-[1,3]dioxolo[4,5-c]pyrrol-4-yl)-2-trityloxy-ethanol

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Technology Process of (S)-1-((3aS,4S,6S,6aR)-2,2,6-Trimethyl-5-nonyl-tetrahydro-[1,3]dioxolo[4,5-c]pyrrol-4-yl)-2-trityloxy-ethanol

There total 3 articles about (S)-1-((3aS,4S,6S,6aR)-2,2,6-Trimethyl-5-nonyl-tetrahydro-[1,3]dioxolo[4,5-c]pyrrol-4-yl)-2-trityloxy-ethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: [2S,3R,4S,5S,(1'R)]-2-methyl-3,4-isopropylidenedioxy-5-(2-triphenylmethyloxy-1-hydroxyethyl)pyrrolidine acetate salt

: 124-19-6
nonan-1-al

: 934347-01-0
(S)-1-((3aS,4S,6S,6aR)-2,2,6-Trimethyl-5-nonyl-tetrahydro-[1,3]dioxolo[4,5-c]pyrrol-4-yl)-2-trityloxy-ethanol

Guidance literature:: With methanol; hydrogen; acetic acid; palladium on activated charcoal;
DOI:10.1021/ol061071r

Reference yield:

: 1-α-methyl-2,3-O-isopropylidene-5-O-methanesulfonyl-6-O-triphenylmethyl-D-mannose

: 934347-01-0
(S)-1-((3aS,4S,6S,6aR)-2,2,6-Trimethyl-5-nonyl-tetrahydro-[1,3]dioxolo[4,5-c]pyrrol-4-yl)-2-trityloxy-ethanol

Guidance literature:: Multi-step reaction with 3 steps

1: 42 percent / NH₃ / ethanol; H₂O / 20 °C

2: 78 percent / H₂ / palladium-carbon

3: 73 percent / MeOH; AcOH; H₂ / palladium-carbon

With methanol; ammonia; hydrogen; acetic acid; palladium on activated charcoal; In ethanol; water;
DOI:10.1021/ol061071r

Reference yield:

: 909703-33-9
1-methyl-2,3-O-isopropylidene-6-O-triphenylmethyl-1,4-dideoxy-1,4-imino-1-N-dehydro-L-allitol

: 934347-01-0
(S)-1-((3aS,4S,6S,6aR)-2,2,6-Trimethyl-5-nonyl-tetrahydro-[1,3]dioxolo[4,5-c]pyrrol-4-yl)-2-trityloxy-ethanol

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / H₂ / palladium-carbon

2: 73 percent / MeOH; AcOH; H₂ / palladium-carbon

With methanol; hydrogen; acetic acid; palladium on activated charcoal;
DOI:10.1021/ol061071r