3-chloro-2-(3-hydroxypropyl)phenyl diethylcarbamate.

Base Information

Chemical Name:3-chloro-2-(3-hydroxypropyl)phenyl diethylcarbamate.
CAS No.:1154740-51-8
Molecular Formula:C₁₄H₂₀ClNO₃
Molecular Weight:285.771
Hs Code.:

Synonyms:3-chloro-2-(3-hydroxypropyl)phenyl diethylcarbamate.

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Chemical Property of 3-chloro-2-(3-hydroxypropyl)phenyl diethylcarbamate.

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Technology Process of 3-chloro-2-(3-hydroxypropyl)phenyl diethylcarbamate.

There total 5 articles about 3-chloro-2-(3-hydroxypropyl)phenyl diethylcarbamate. which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 1154740-50-7
C₁₄H₁₆ClNO₃

: 1154740-51-8
3-chloro-2-(3-hydroxypropyl)phenyl diethylcarbamate.

Guidance literature:: With hydrogen; Rh/Al₂O₃; In ethyl acetate; at 20 ℃; under 760.051 Torr;

Reference yield:

: 863870-77-3
3-chloro-2-iodophenyl N,N-dimethyl O-carbamate

: 1154740-51-8
3-chloro-2-(3-hydroxypropyl)phenyl diethylcarbamate.

Guidance literature:: Multi-step reaction with 2 steps

1: diisopropylamine / copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1 h / 100 °C

2: hydrogen / rhodium nanoparticles supported on γ-alumina / ethyl acetate / 20 °C / 760.05 Torr

With hydrogen; diisopropylamine; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; rhodium nanoparticles supported on γ-alumina; In ethyl acetate;

Reference yield:

: 108-43-0
3-monochlorophenol

: 1154740-51-8
3-chloro-2-(3-hydroxypropyl)phenyl diethylcarbamate.

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydride / tetrahydrofuran / 1 h / 20 °C

1.2: 20 °C

2.1: lithium diisopropyl amide / tetrahydrofuran; hexanes / 0.5 h / -78 °C

2.2: 2.5 h / -78 - 20 °C

3.1: diisopropylamine / copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1 h / 100 °C

4.1: hydrogen / rhodium nanoparticles supported on γ-alumina / ethyl acetate / 20 °C / 760.05 Torr

With hydrogen; sodium hydride; diisopropylamine; lithium diisopropyl amide; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; rhodium nanoparticles supported on γ-alumina; In tetrahydrofuran; hexanes; ethyl acetate;