C₃₃H₃₇N₃O₅S₂

Base Information

Chemical Name:C₃₃H₃₇N₃O₅S₂
CAS No.:1383385-82-7
Molecular Formula:C₃₃H₃₇N₃O₅S₂
Molecular Weight:619.806
Hs Code.:

C<sub>33</sub>H<sub>37</sub>N<sub>3</sub>O<sub>5</sub>S<sub>2</sub>

Synonyms:C₃₃H₃₇N₃O₅S₂

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Chemical Property of C₃₃H₃₇N₃O₅S₂

Chemical Property:

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Technology Process of C₃₃H₃₇N₃O₅S₂

There total 14 articles about C₃₃H₃₇N₃O₅S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3973-08-8
Thiazole-4-carboxylic acid

: 1383385-81-6
C₃₄H₄₄N₂O₆S

: 1383385-82-7
C₃₃H₃₇N₃O₅S₂

Guidance literature:: C₃₄H₄₄N₂O₆S; With trifluoroacetic acid; In dichloromethane; at 20 ℃; Inert atmosphere;

Thiazole-4-carboxylic acid; With triethylamine; HATU; In N,N-dimethyl-formamide; at 20 ℃; for 15h;

Reference yield:

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 1383385-82-7
C₃₃H₃₇N₃O₅S₂

Guidance literature:: Multi-step reaction with 12 steps

1.1: sodium hexamethyldisilazane / tetrahydrofuran / 8 h / -78 °C / Inert atmosphere

2.1: sodium carbonate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / N,N-dimethyl-formamide; water / 4 h / 90 °C / Inert atmosphere

3.1: n-butyllithium / tetrahydrofuran / 0.5 h / -78 °C

3.2: 2 h / -78 - 20 °C

4.1: sodium carbonate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / water / 2 h / 80 °C / Inert atmosphere

5.1: hydrogen / palladium 10% on activated carbon / methanol / 15 h / 2585.81 Torr

6.1: acetonitrile / 3 h / 80 °C

7.1: sodium tetrahydroborate / methanol / 1 h

8.1: lithium diisopropyl amide / n-heptane; tetrahydrofuran; ethylbenzene / 2.5 h / -78 °C / Inert atmosphere

8.2: 1.5 h / -78 °C

9.1: carbonochloridic acid 1-chloro-ethyl ester / 1,2-dichloro-ethane / 4 h / Reflux

10.1: dmap; triethylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 15 h / 20 °C

11.1: sodium carbonate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / N,N-dimethyl-formamide; water / 4 h / 92 °C / Inert atmosphere

12.1: trifluoroacetic acid / dichloromethane / 20 °C / Inert atmosphere

12.2: 15 h / 20 °C

With dmap; sodium tetrahydroborate; n-butyllithium; carbonochloridic acid 1-chloro-ethyl ester; hydrogen; sodium hexamethyldisilazane; sodium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trifluoroacetic acid; lithium diisopropyl amide; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; palladium 10% on activated carbon; In tetrahydrofuran; methanol; n-heptane; dichloromethane; ethylbenzene; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 22288-78-4
Methyl 3-aminothiophene-2-carboxylate

: 1383385-82-7
C₃₃H₃₇N₃O₅S₂

Guidance literature:: Multi-step reaction with 10 steps

1.1: diiodomethane; tert.-butylnitrite / acetonitrile / 1.5 h / 50 °C

2.1: sodium carbonate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / water / 2 h / 80 °C / Inert atmosphere

3.1: hydrogen / palladium 10% on activated carbon / methanol / 15 h / 2585.81 Torr

4.1: acetonitrile / 3 h / 80 °C

5.1: sodium tetrahydroborate / methanol / 1 h

6.1: lithium diisopropyl amide / n-heptane; tetrahydrofuran; ethylbenzene / 2.5 h / -78 °C / Inert atmosphere

6.2: 1.5 h / -78 °C

7.1: carbonochloridic acid 1-chloro-ethyl ester / 1,2-dichloro-ethane / 4 h / Reflux

8.1: dmap; triethylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 15 h / 20 °C

9.1: sodium carbonate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / N,N-dimethyl-formamide; water / 4 h / 92 °C / Inert atmosphere

10.1: trifluoroacetic acid / dichloromethane / 20 °C / Inert atmosphere

10.2: 15 h / 20 °C

With dmap; sodium tetrahydroborate; tert.-butylnitrite; diiodomethane; carbonochloridic acid 1-chloro-ethyl ester; hydrogen; sodium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trifluoroacetic acid; lithium diisopropyl amide; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; palladium 10% on activated carbon; In tetrahydrofuran; methanol; n-heptane; dichloromethane; ethylbenzene; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetonitrile;