(2-propargyloxyphenyl)bis(pyrazolyl)methane

Base Information

Chemical Name:(2-propargyloxyphenyl)bis(pyrazolyl)methane
CAS No.:926645-82-1
Molecular Formula:C₁₆H₁₄N₄O
Molecular Weight:278.313
Hs Code.:

Synonyms:(2-propargyloxyphenyl)bis(pyrazolyl)methane

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Chemical Property of (2-propargyloxyphenyl)bis(pyrazolyl)methane

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Technology Process of (2-propargyloxyphenyl)bis(pyrazolyl)methane

There total 1 articles about (2-propargyloxyphenyl)bis(pyrazolyl)methane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: (2-hydroxyphenyl)bis(pyrazol-1-yl)methane

: 106-96-7
propargyl bromide

: 926645-82-1
(2-propargyloxyphenyl)bis(pyrazolyl)methane

Guidance literature:: With potassium carbonate; In acetone; for 8h; Heating;
DOI:10.1039/b613311h

Reference yield: 92.0%

: 926645-82-1
(2-propargyloxyphenyl)bis(pyrazolyl)methane

: 14243-64-2
(triphenylphosphine)gold(I) chloride

: [(pyrazolyl)2CH(C₆H₄-2-OCH₂CCAuPPh₃]

Guidance literature:: With KOH; In methanol; mixt. was stirred for ca. 18 h; soln. was evapd. to dryness, solid was extd. into CH2Cl2, extract was passed through Celite and concd. in vac., Et2O was added, ppt. was isolated by filtration, dried; elem. anal.;
DOI:10.1039/b613311h

Reference yield: 92.0%

: 926645-82-1
(2-propargyloxyphenyl)bis(pyrazolyl)methane

: 7732-18-5
water

: copper(II) nitrate

: [Cu((2-propargyloxyphenyl)bis(pyrazolyl)methane)2](NO₃)2*2H₂O

Guidance literature:: In ethanol; acetone; to soln. of metal nitrate in EtOH was added soln. of ligand in acetone, mixt. was left to stand in open vessel and crystals were deposited aftera few days; ppt. was collected on frit, washed with EtOH and Et2O, dried in vac.; elem. anal.;
DOI:10.1039/b613311h