Technology Process of 4-(4'-Methylphenyl)-4-pentenal
There total 12 articles about 4-(4'-Methylphenyl)-4-pentenal which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tartaric acid;
In
dichloromethane;
at 25 ℃;
for 75h;
Yield given;
DOI:10.1021/ja00084a025
- Guidance literature:
-
Multi-step reaction with 3 steps
1: p-toluenesulfonic acid monohydrate / methanol
2: NiCl2(dppp) / diethyl ether / 17 h / Heating
3: 15percent tartaric acid / CH2Cl2 / 75 h / 25 °C
With
1,3-bis[(diphenylphosphino)propane]dichloronickel(II); toluene-4-sulfonic acid; tartaric acid;
In
methanol; diethyl ether; dichloromethane;
DOI:10.1021/ja00084a025
- Guidance literature:
-
Multi-step reaction with 2 steps
1: NiCl2(dppp) / diethyl ether / 17 h / Heating
2: 15percent tartaric acid / CH2Cl2 / 75 h / 25 °C
With
1,3-bis[(diphenylphosphino)propane]dichloronickel(II); tartaric acid;
In
diethyl ether; dichloromethane;
DOI:10.1021/ja00084a025
