(CH₃)4N⁽¹⁺⁾*(CO)4Re(C₆H₅)(⁽¹³⁾COCH₃)^(1-)

Base Information

Chemical Name:(CH₃)4N⁽¹⁺⁾*(CO)4Re(C₆H₅)(⁽¹³⁾COCH₃)^(1-)
CAS No.:83207-79-8
Molecular Formula:C₄H₁₂N*C₁₂H₈O₅Re
Molecular Weight:493.534
Hs Code.:

(CH<sub>3</sub>)4N<sup>(1+)</sup>*(CO)4Re(C<sub>6</sub>H<sub>5</sub>)(<sup>(13)</sup>COCH<sub>3</sub>)<sup>(1-)</sup>

Synonyms:(CH₃)4N⁽¹⁺⁾*(CO)4Re(C₆H₅)(⁽¹³⁾COCH₃)^(1-)

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Chemical Property of (CH₃)4N⁽¹⁺⁾*(CO)4Re(C₆H₅)(⁽¹³⁾COCH₃)^(1-)

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Technology Process of (CH₃)4N⁽¹⁺⁾*(CO)4Re(C₆H₅)(⁽¹³⁾COCH₃)^(1-)

There total 3 articles about (CH₃)4N⁽¹⁺⁾*(CO)4Re(C₆H₅)(⁽¹³⁾COCH₃)^(1-) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 83207-85-6
cis-(CO)4Re(⁽¹³⁾CO)C₆H₅

: 917-54-4
methyllithium

: 75-57-0
tetramethlyammonium chloride

: 83207-79-8
(CH₃)4N⁽¹⁺⁾*(CO)4Re(C₆H₅)(⁽¹³⁾COCH₃)^(1-)

: 83247-86-3
(CH₃)4N⁽¹⁺⁾*(CO)3(⁽¹³⁾CO)Re(C₆H₅)(COCH₃)^(1-)

: 83247-88-5
(CH₃)4N⁽¹⁺⁾*(CO)3(⁽¹³⁾CO)Re(C₆H₅)(COCH₃)^(1-)

: 83207-81-2
(CH₃)4N⁽¹⁺⁾*(CO)3(⁽¹³⁾CO)Re(C₆H₅)(COCH₃)^(1-)

: (CH₃)4N⁽¹⁺⁾*(CO)4Re(C₆H₅)(COCH₃)^(1-)

Guidance literature:: In tetrahydrofuran; byproducts: LiCl; CH3Li was added to a soln. of complex in THF at -78°C, stirred at this temp. for 1 h, warmed to room temp., H2O was added, filtered, evapd., N(CH3)4Cl in CH2Cl2 was added;; CH2Cl2 layer was sepd., evapd., dissolved in THF, filtered, evapd., washed with ether and dried under vac.; labeled isomers were detected by NMR spectra;;
DOI:10.1021/ja00387a032

Reference yield: 19.0%

: 83207-73-2
(CH₃)4N⁽¹⁺⁾*(CO)4Re(⁽¹³⁾COCH₃)COC₆H₅^(1-)

: 83207-79-8
(CH₃)4N⁽¹⁺⁾*(CO)4Re(C₆H₅)(⁽¹³⁾COCH₃)^(1-)

: 83247-86-3
(CH₃)4N⁽¹⁺⁾*(CO)3(⁽¹³⁾CO)Re(C₆H₅)(COCH₃)^(1-)

: 83247-88-5
(CH₃)4N⁽¹⁺⁾*(CO)3(⁽¹³⁾CO)Re(C₆H₅)(COCH₃)^(1-)

: 83207-81-2
(CH₃)4N⁽¹⁺⁾*(CO)3(⁽¹³⁾CO)Re(C₆H₅)(COCH₃)^(1-)

: 65583-19-9
(CH₃)4N⁽¹⁺⁾*(CO)4Re(CH₃)(COC₆H₅)^(1-)

Guidance literature:: With Λ-(+)-tris(acetylacetonato)chromium(III); In [⁽²⁾H₆]acetone; Thermolysis of acetone-d6 soln. at 68.6°C for 1 h;; not sepd., detected by 13C NMR spectra;;
DOI:10.1021/ja00387a032

Reference yield: 17.0%

: 83207-77-6
(CH₃)4N⁽¹⁺⁾*(CO)3(⁽¹³⁾CO)Re(COCH₃)COC₆H₅^(1-)

: 83207-79-8
(CH₃)4N⁽¹⁺⁾*(CO)4Re(C₆H₅)(⁽¹³⁾COCH₃)^(1-)

: 83247-86-3
(CH₃)4N⁽¹⁺⁾*(CO)3(⁽¹³⁾CO)Re(C₆H₅)(COCH₃)^(1-)

: 83247-88-5
(CH₃)4N⁽¹⁺⁾*(CO)3(⁽¹³⁾CO)Re(C₆H₅)(COCH₃)^(1-)

: 83207-81-2
(CH₃)4N⁽¹⁺⁾*(CO)3(⁽¹³⁾CO)Re(C₆H₅)(COCH₃)^(1-)

Guidance literature:: With Λ-(+)-tris(acetylacetonato)chromium(III); In [⁽²⁾H₆]acetone; Thermolysis of acetone-d6 soln. at 68.6°C for 1 h;; not sepd., detected by 13C NMR spectra;;
DOI:10.1021/ja00387a032