N-(6-bromo-3,4-dimethoxy)benzyl isatin

Base Information

Chemical Name:N-(6-bromo-3,4-dimethoxy)benzyl isatin
CAS No.:1394134-40-7
Molecular Formula:C₁₇H₁₄BrNO₄
Molecular Weight:376.206
Hs Code.:

Synonyms:N-(6-bromo-3,4-dimethoxy)benzyl isatin

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Chemical Property of N-(6-bromo-3,4-dimethoxy)benzyl isatin

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Technology Process of N-(6-bromo-3,4-dimethoxy)benzyl isatin

There total 2 articles about N-(6-bromo-3,4-dimethoxy)benzyl isatin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 53207-00-4
1-bromo-2-(bromomethyl)-4,5-dimethoxybenzene

: 91-56-5,1186480-61-4,84788-92-1
indole-2,3-dione

: 1394134-40-7
N-(6-bromo-3,4-dimethoxy)benzyl isatin

Guidance literature:: indole-2,3-dione; With sodium hydride; In N,N-dimethyl-formamide; at 0 ℃; for 0.333333h; Inert atmosphere;

1-bromo-2-(bromomethyl)-4,5-dimethoxybenzene; In N,N-dimethyl-formamide; at 0 - 23 ℃; Inert atmosphere;
DOI:10.1021/ol3019677

Reference yield:

: 54370-00-2
2-bromo-4,5-dimethoxybenzyl alcohol

: 1394134-40-7
N-(6-bromo-3,4-dimethoxy)benzyl isatin

Guidance literature:: Multi-step reaction with 2 steps

1.1: phosphorus tribromide / diethyl ether / 0.83 h / 0 - 23 °C / Inert atmosphere

2.1: sodium hydride / N,N-dimethyl-formamide / 0.33 h / 0 °C / Inert atmosphere

2.2: 0 - 23 °C / Inert atmosphere

With phosphorus tribromide; sodium hydride; In diethyl ether; N,N-dimethyl-formamide;
DOI:10.1021/ol3019677