prop-2-en-1-yl 2,3-di-O-benzoyl-4-O-[tertbutyl(dimethyl)silyl]-6-methyl-β-D-glucopyranuronosyl-(1→3)-4,6-O-benzylidene-2-deoxy-2-{[(2,2,2-trichloroethoxy)carbonyl]-amino}-β-D-glucopyranosyl-(1→4)-2,3-di-O-benzoyl-6-methyl-β-D-glucopyranuronosyl-(1→3)-2-(acetylamino)-4,6-O-benzylidene-2-deoxy-α-D-glucopyranoside

Base Information

Chemical Name:prop-2-en-1-yl 2,3-di-O-benzoyl-4-O-[tertbutyl(dimethyl)silyl]-6-methyl-β-D-glucopyranuronosyl-(1→3)-4,6-O-benzylidene-2-deoxy-2-{[(2,2,2-trichloroethoxy)carbonyl]-amino}-β-D-glucopyranosyl-(1→4)-2,3-di-O-benzoyl-6-methyl-β-D-glucopyranuronosyl-(1→3)-2-(acetylamino)-4,6-O-benzylidene-2-deoxy-α-D-glucopyranoside
CAS No.:1419710-86-3
Molecular Formula:C₈₂H₈₉Cl₃N₂O₂₈Si
Molecular Weight:1685.05
Hs Code.:

prop-2-en-1-yl 2,3-di-O-benzoyl-4-O-[tertbutyl(dimethyl)silyl]-6-methyl-β-D-glucopyranuronosyl-(1→3)-4,6-O-benzylidene-2-deoxy-2-{[(2,2,2-trichloroethoxy)carbonyl]-amino}-β-D-glucopyranosyl-(1→4)-2,3-di-O-benzoyl-6-methyl-β-D-glucopyranuronosyl-(1→3)-2-(acetylamino)-4,6-O-benzylidene-2-deoxy-α-D-glucopyranoside

Synonyms:prop-2-en-1-yl 2,3-di-O-benzoyl-4-O-[tertbutyl(dimethyl)silyl]-6-methyl-β-D-glucopyranuronosyl-(1→3)-4,6-O-benzylidene-2-deoxy-2-{[(2,2,2-trichloroethoxy)carbonyl]-amino}-β-D-glucopyranosyl-(1→4)-2,3-di-O-benzoyl-6-methyl-β-D-glucopyranuronosyl-(1→3)-2-(acetylamino)-4,6-O-benzylidene-2-deoxy-α-D-glucopyranoside

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Chemical Property of prop-2-en-1-yl 2,3-di-O-benzoyl-4-O-[tertbutyl(dimethyl)silyl]-6-methyl-β-D-glucopyranuronosyl-(1→3)-4,6-O-benzylidene-2-deoxy-2-{[(2,2,2-trichloroethoxy)carbonyl]-amino}-β-D-glucopyranosyl-(1→4)-2,3-di-O-benzoyl-6-methyl-β-D-glucopyranuronosyl-(1→3)-2-(acetylamino)-4,6-O-benzylidene-2-deoxy-α-D-glucopyranoside

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Technology Process of prop-2-en-1-yl 2,3-di-O-benzoyl-4-O-[tertbutyl(dimethyl)silyl]-6-methyl-β-D-glucopyranuronosyl-(1→3)-4,6-O-benzylidene-2-deoxy-2-{[(2,2,2-trichloroethoxy)carbonyl]-amino}-β-D-glucopyranosyl-(1→4)-2,3-di-O-benzoyl-6-methyl-β-D-glucopyranuronosyl-(1→3)-2-(acetylamino)-4,6-O-benzylidene-2-deoxy-α-D-glucopyranoside

There total 1 articles about prop-2-en-1-yl 2,3-di-O-benzoyl-4-O-[tertbutyl(dimethyl)silyl]-6-methyl-β-D-glucopyranuronosyl-(1→3)-4,6-O-benzylidene-2-deoxy-2-{[(2,2,2-trichloroethoxy)carbonyl]-amino}-β-D-glucopyranosyl-(1→4)-2,3-di-O-benzoyl-6-methyl-β-D-glucopyranuronosyl-(1→3)-2-(acetylamino)-4,6-O-benzylidene-2-deoxy-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 4-methylphenyl 4,6-O-benzylidene-2-deoxy-3-O-{2,3-di-O-benzoyl-4-O-[tert-butyl-(dimethyl)silyl]-6-methyl-β-D-glucopyranuronosyl}-1-thio-2-{[(2,2,2-trichloroethoxy)-carbonyl]amino}-β-D-glucopyranoside

: 1419710-81-8
prop-2-en-1-yl 2-(acetylamino)-4,6-O-benzylidene-2-deoxy-3-O-(2,3-di-O-benzoyl-6-methyl-β-D-glucopyranosyl)-α-D-glucopyranoside

: 1419710-86-3
prop-2-en-1-yl 2,3-di-O-benzoyl-4-O-[tertbutyl(dimethyl)silyl]-6-methyl-β-D-glucopyranuronosyl-(1→3)-4,6-O-benzylidene-2-deoxy-2-{[(2,2,2-trichloroethoxy)carbonyl]-amino}-β-D-glucopyranosyl-(1→4)-2,3-di-O-benzoyl-6-methyl-β-D-glucopyranuronosyl-(1→3)-2-(acetylamino)-4,6-O-benzylidene-2-deoxy-α-D-glucopyranoside

Guidance literature:: 4-methylphenyl 4,6-O-benzylidene-2-deoxy-3-O-{2,3-di-O-benzoyl-4-O-[tert-butyl-(dimethyl)silyl]-6-methyl-β-D-glucopyranuronosyl}-1-thio-2-{[(2,2,2-trichloroethoxy)-carbonyl]amino}-β-D-glucopyranoside; prop-2-en-1-yl 2-(acetylamino)-4,6-O-benzylidene-2-deoxy-3-O-(2,3-di-O-benzoyl-6-methyl-β-D-glucopyranosyl)-α-D-glucopyranoside; With N-iodo-succinimide; In dichloromethane; at 20 ℃; for 1h; Molecular sieve; Inert atmosphere;

With trifluorormethanesulfonic acid; In dichloromethane; at 20 ℃; for 16h; Inert atmosphere; Molecular sieve;
DOI:10.1016/j.bmc.2012.11.025