2-tert-butyl 12a-methyl (4aS,12aR)-1,2,3,4,4a,5,12,12a-octahydro-9-phenylpyrido[3,4-b]acridine-2,12a-dicarboxylate

Base Information

Chemical Name:2-tert-butyl 12a-methyl (4aS,12aR)-1,2,3,4,4a,5,12,12a-octahydro-9-phenylpyrido[3,4-b]acridine-2,12a-dicarboxylate
CAS No.:1059572-95-0
Molecular Formula:C₂₉H₃₂N₂O₄
Molecular Weight:472.584
Hs Code.:

Synonyms:2-tert-butyl 12a-methyl (4aS,12aR)-1,2,3,4,4a,5,12,12a-octahydro-9-phenylpyrido[3,4-b]acridine-2,12a-dicarboxylate

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Chemical Property of 2-tert-butyl 12a-methyl (4aS,12aR)-1,2,3,4,4a,5,12,12a-octahydro-9-phenylpyrido[3,4-b]acridine-2,12a-dicarboxylate

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Technology Process of 2-tert-butyl 12a-methyl (4aS,12aR)-1,2,3,4,4a,5,12,12a-octahydro-9-phenylpyrido[3,4-b]acridine-2,12a-dicarboxylate

There total 1 articles about 2-tert-butyl 12a-methyl (4aS,12aR)-1,2,3,4,4a,5,12,12a-octahydro-9-phenylpyrido[3,4-b]acridine-2,12a-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1059572-89-2
2-tert-butyl 12a-methyl (4aS,12aR)-9-bromo-1,2,3,4,4a,5,12,12a-octahydropyrido[3,4-b]acridine-2,12a-dicarboxylate

: 98-80-6
phenylboronic acid

: 1059572-95-0
2-tert-butyl 12a-methyl (4aS,12aR)-1,2,3,4,4a,5,12,12a-octahydro-9-phenylpyrido[3,4-b]acridine-2,12a-dicarboxylate

Guidance literature:: With sodium tetrachloropalladate(II); dicyclohexyl {2-sulfo-9-[3-(4-sulfophenyl)propyl]-9H-fluoren-9-yl}phosphonium hydrogen sulfate; potassium carbonate; In water; butan-1-ol; at 100 ℃; for 16h;
DOI:10.1055/s-2008-1067148