N-(3-methoxy-benzyl)-N-methyl-2-(3,5-dichlorophenyl)-2-(phenylsulfanyl)-acetamide

Base Information

Chemical Name:N-(3-methoxy-benzyl)-N-methyl-2-(3,5-dichlorophenyl)-2-(phenylsulfanyl)-acetamide
CAS No.:929048-76-0
Molecular Formula:C₂₃H₂₁Cl₂NO₂S
Molecular Weight:446.397
Hs Code.:

Synonyms:N-(3-methoxy-benzyl)-N-methyl-2-(3,5-dichlorophenyl)-2-(phenylsulfanyl)-acetamide

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Chemical Property of N-(3-methoxy-benzyl)-N-methyl-2-(3,5-dichlorophenyl)-2-(phenylsulfanyl)-acetamide

Chemical Property:

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Technology Process of N-(3-methoxy-benzyl)-N-methyl-2-(3,5-dichlorophenyl)-2-(phenylsulfanyl)-acetamide

There total 6 articles about N-(3-methoxy-benzyl)-N-methyl-2-(3,5-dichlorophenyl)-2-(phenylsulfanyl)-acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 929048-75-9
2-(3,5-dichlorophenyl)-2-(phenylsulfanyl)-acetic acid

: 41789-95-1
1-(3-methoxyphenyl)-N-methylmethanamine

: 929048-76-0
N-(3-methoxy-benzyl)-N-methyl-2-(3,5-dichlorophenyl)-2-(phenylsulfanyl)-acetamide

Guidance literature:: 2-(3,5-dichlorophenyl)-2-(phenylsulfanyl)-acetic acid; With 1,1'-carbonyldiimidazole; In dichloromethane; at 20 ℃; for 2h;

1-(3-methoxyphenyl)-N-methylmethanamine; In dichloromethane; for 1h;

Reference yield:

: 2-(3,5-dichlorophenyl)-2-hydroxyacetic acid

: 929048-76-0
N-(3-methoxy-benzyl)-N-methyl-2-(3,5-dichlorophenyl)-2-(phenylsulfanyl)-acetamide

Guidance literature:: Multi-step reaction with 5 steps

1.1: hydrogenchloride / 20 h / 20 °C

2.1: triethylamine / dichloromethane / 3 h / 0 - 20 °C

3.1: potassium bromide / N,N-dimethyl-formamide / 1.5 h / 50 °C

4.1: potassium hydroxide / 1,4-dioxane / 1 h / 90 °C

4.2: 2 h / 20 °C / Heating / reflux

5.1: 1,1'-carbonyldiimidazole / dichloromethane / 2 h / 20 °C

5.2: 1 h

With hydrogenchloride; potassium hydroxide; triethylamine; 1,1'-carbonyldiimidazole; potassium bromide; In 1,4-dioxane; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 929048-72-6
methyl 2-bromo-2-(3,5-dichlorophenyl)acetate

: 929048-76-0
N-(3-methoxy-benzyl)-N-methyl-2-(3,5-dichlorophenyl)-2-(phenylsulfanyl)-acetamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium hydroxide / 1,4-dioxane / 1 h / 90 °C

1.2: 2 h / 20 °C / Heating / reflux

2.1: 1,1'-carbonyldiimidazole / dichloromethane / 2 h / 20 °C

2.2: 1 h

With potassium hydroxide; 1,1'-carbonyldiimidazole; In 1,4-dioxane; dichloromethane;