(6S)-benzyl 6-<(S)-2-amino-2-phenylacetamido>-6-(methylthio)penicillanate

Base Information

Chemical Name:(6S)-benzyl 6-<(S)-2-amino-2-phenylacetamido>-6-(methylthio)penicillanate
CAS No.:111821-11-5
Molecular Formula:C₂₄H₂₇N₃O₄S₂
Molecular Weight:485.628
Hs Code.:

Synonyms:(6S)-benzyl 6-<(S)-2-amino-2-phenylacetamido>-6-(methylthio)penicillanate

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Chemical Property of (6S)-benzyl 6-<(S)-2-amino-2-phenylacetamido>-6-(methylthio)penicillanate

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Technology Process of (6S)-benzyl 6-<(S)-2-amino-2-phenylacetamido>-6-(methylthio)penicillanate

There total 4 articles about (6S)-benzyl 6-<(S)-2-amino-2-phenylacetamido>-6-(methylthio)penicillanate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

: 111761-69-4
(6S)-benzyl 6-<(R)-2-azido-2-phenylacetamido>-6-(methylthio)penicillanate

: 111821-10-4
(6S)-benzyl 6-<(R)-2-amino-2-phenylacetamido>-6-(methylthio)penicillanate

: 111821-11-5
(6S)-benzyl 6-<(S)-2-amino-2-phenylacetamido>-6-(methylthio)penicillanate

Guidance literature:: With hydrogen sulfide; triethylamine; In dichloromethane; for 0.5h; Ambient temperature;
DOI:10.1039/P19870000635

Reference yield:

: 40514-98-5
(6S)-benzyl 6-amino-6-(methylthio)penicillanate

: 111821-11-5
(6S)-benzyl 6-<(S)-2-amino-2-phenylacetamido>-6-(methylthio)penicillanate

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / triethylamine / tetrahydrofuran / 0.5 h / Ambient temperature

2: 31 percent / triethylamine, H₂S gas / CH₂Cl₂ / 0.5 h / Ambient temperature

With hydrogen sulfide; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1039/P19870000635

Reference yield:

: 29125-25-5,3380-95-8
(R)-2-azido-2-phenylacetic acid

: 111821-11-5
(6S)-benzyl 6-<(S)-2-amino-2-phenylacetamido>-6-(methylthio)penicillanate

Guidance literature:: Multi-step reaction with 3 steps

1: oxalyl chloride, dry DMF / CH₂Cl₂ / 1 h / Ambient temperature

2: 92 percent / triethylamine / tetrahydrofuran / 0.5 h / Ambient temperature

3: 31 percent / triethylamine, H₂S gas / CH₂Cl₂ / 0.5 h / Ambient temperature

With oxalyl dichloride; hydrogen sulfide; triethylamine; N,N-dimethyl-formamide; In tetrahydrofuran; dichloromethane;
DOI:10.1039/P19870000635