p-tolyl 2,3,5,6-tetra-O-benzoyl-β-D-galactofuranosyl-(1->6)-2,3,5-tri-O-benzoyl-1-thio-β-D-galactofuranoside

Base Information

• Chemical Name: p-tolyl 2,3,5,6-tetra-O-benzoyl-β-D-galactofuranosyl-(1->6)-2,3,5-tri-O-benzoyl-1-thio-β-D-galactofuranoside
• CAS No.: 1033561-11-3
• Molecular Formula: C₆₈H₅₆O₁₇S
• Molecular Weight: 1177.25

Synonyms:p-tolyl 2,3,5,6-tetra-O-benzoyl-β-D-galactofuranosyl-(1->6)-2,3,5-tri-O-benzoyl-1-thio-β-D-galactofuranoside

Chemical Property of p-tolyl 2,3,5,6-tetra-O-benzoyl-β-D-galactofuranosyl-(1->6)-2,3,5-tri-O-benzoyl-1-thio-β-D-galactofuranoside

Chemical Property:

Purity/Quality:

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Technology Process of p-tolyl 2,3,5,6-tetra-O-benzoyl-β-D-galactofuranosyl-(1->6)-2,3,5-tri-O-benzoyl-1-thio-β-D-galactofuranoside

There total 1 articles about p-tolyl 2,3,5,6-tetra-O-benzoyl-β-D-galactofuranosyl-(1->6)-2,3,5-tri-O-benzoyl-1-thio-β-D-galactofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

p-tolyl 2,3,5-tri-O-benzoyl-1-thio-β-D-galactofuranoside (1033560-54-1) + O-(2,3,5,6-tetra-O-benzoyl-D-galactofuranosyl) trichloroacetimidate (1033561-09-9) → p-tolyl 2,3,5,6-tetra-O-benzoyl-β-D-galactofuranosyl-(1->6)-2,3,5-tri-O-benzoyl-1-thio-β-D-galactofuranoside (1033561-11-3)

Guidance literature:

With trimethylsilyl trifluoromethanesulfonate; 4 A molecular sieve; In dichloromethane; for 1h;

DOI:10.1021/jo800457j

Reference yield: 74.0%

p-tolyl 2,3,5,6-tetra-O-benzoyl-β-D-galactofuranosyl-(1->6)-2,3,5-tri-O-benzoyl-1-thio-β-D-galactofuranoside (1033561-11-3) → 2,3,5,6-tetra-O-benzoyl-β-D-galactofuranosyl-(1->6)-2,3,5-tri-O-benzoyl-D-galactofuranose (124662-86-8)

Guidance literature:

With N-Bromosuccinimide; water; In ethyl acetate; for 4h;

DOI:10.1021/jo800457j

Reference yield:

p-tolyl 2,3,5,6-tetra-O-benzoyl-β-D-galactofuranosyl-(1->6)-2,3,5-tri-O-benzoyl-1-thio-β-D-galactofuranoside (1033561-11-3) + octyl 2,3,6-tri-O-benzoyl-β-D-galactofuranoside (396716-63-5) → octyl 2,3,5,6-tri-O-benzoyl-β-D-galactofuranosyl-(1->6)-2,3,5-tri-O-benzoyl-β-D-galactofuranosyl)-(1->5)-2,3,6-tri-O-benzoyl-β-D-galactofuranoside (1033560-85-8)

Guidance literature:

With N-iodo-succinimide; silver trifluoromethanesulfonate; In dichloromethane; for 0.5h;

DOI:10.1021/jo800457j

upstream raw materials:

p-tolyl 2,3,5-tri-O-benzoyl-1-thio-β-D-galactofuranoside

O-(2,3,5,6-tetra-O-benzoyl-D-galactofuranosyl) trichloroacetimidate

Downstream raw materials:

2,3,5,6-tetra-O-benzoyl-β-D-galactofuranosyl-(1->6)-2,3,5-tri-O-benzoyl-D-galactofuranose

octyl 2,3,5,6-tri-O-benzoyl-β-D-galactofuranosyl-(1->6)-2,3,5-tri-O-benzoyl-β-D-galactofuranosyl)-(1->5)-2,3,6-tri-O-benzoyl-β-D-galactofuranoside

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