3-O-(4',5',6',8'-tetra-O-benzyl-1',2'-dideoxy-α-D-gluco-oct-1'-eno-3'-ulopyranosyl)-5,6-dideoxy-1,2-O-isopropylidene-α-D-xylo-hex-5-enofuranoside

Base Information

Chemical Name:3-O-(4',5',6',8'-tetra-O-benzyl-1',2'-dideoxy-α-D-gluco-oct-1'-eno-3'-ulopyranosyl)-5,6-dideoxy-1,2-O-isopropylidene-α-D-xylo-hex-5-enofuranoside
CAS No.:709654-98-8
Molecular Formula:C₄₅H₅₀O₉
Molecular Weight:734.887
Hs Code.:

Synonyms:3-O-(4',5',6',8'-tetra-O-benzyl-1',2'-dideoxy-α-D-gluco-oct-1'-eno-3'-ulopyranosyl)-5,6-dideoxy-1,2-O-isopropylidene-α-D-xylo-hex-5-enofuranoside

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Chemical Property of 3-O-(4',5',6',8'-tetra-O-benzyl-1',2'-dideoxy-α-D-gluco-oct-1'-eno-3'-ulopyranosyl)-5,6-dideoxy-1,2-O-isopropylidene-α-D-xylo-hex-5-enofuranoside

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Technology Process of 3-O-(4',5',6',8'-tetra-O-benzyl-1',2'-dideoxy-α-D-gluco-oct-1'-eno-3'-ulopyranosyl)-5,6-dideoxy-1,2-O-isopropylidene-α-D-xylo-hex-5-enofuranoside

There total 2 articles about 3-O-(4',5',6',8'-tetra-O-benzyl-1',2'-dideoxy-α-D-gluco-oct-1'-eno-3'-ulopyranosyl)-5,6-dideoxy-1,2-O-isopropylidene-α-D-xylo-hex-5-enofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 7284-07-3
5,6-dideoxy-1,2-O-isopropylidene-α-D-xylo-hex-5-eno-furanose

: 166828-15-5
4,5,6,8-tetra-O-benzyl-1,2-dideoxy-α-D-gluco-oct-1-eno-3-ulopyranose

: 709654-98-8
3-O-(4',5',6',8'-tetra-O-benzyl-1',2'-dideoxy-α-D-gluco-oct-1'-eno-3'-ulopyranosyl)-5,6-dideoxy-1,2-O-isopropylidene-α-D-xylo-hex-5-enofuranoside

Guidance literature:: With 4 A molecular sieve; Montmorillonite K-10 clay; In dichloromethane; at 20 ℃;
DOI:10.1039/b401699h

Reference yield:

: 13096-62-3
(3R,4S,5R,6R)-3,4,5-tris(benzyloxy)-6-((benzyloxy)methyl)tetrahydro-2H-pyran-2-one

: 709654-98-8
3-O-(4',5',6',8'-tetra-O-benzyl-1',2'-dideoxy-α-D-gluco-oct-1'-eno-3'-ulopyranosyl)-5,6-dideoxy-1,2-O-isopropylidene-α-D-xylo-hex-5-enofuranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / diethyl ether / -78 °C

2: 45 percent / Montmorillonite K-10 clay; 4 Angstroem molecular sieves / CH₂Cl₂ / 20 °C

With 4 A molecular sieve; Montmorillonite K-10 clay; In diethyl ether; dichloromethane;
DOI:10.1039/b401699h