,S^)>-β-<<(1,1-dimethylethoxy)carbonyl>amino>-α-cyclohexanepropanol

Base Information

Chemical Name:*,S^*)>-β-<<(1,1-dimethylethoxy)carbonyl>amino>-α-cyclohexanepropanol
CAS No.:151521-07-2
Molecular Formula:C₁₈H₃₅NO₃S₃
Molecular Weight:409.679
Hs Code.:

<R-(R<sup>*</sup>,S<sup>*</sup>)>-β-<<(1,1-dimethylethoxy)carbonyl>amino>-α-<tris(methylthio)methyl>cyclohexanepropanol

Synonyms:*,S^*)>-β-<<(1,1-dimethylethoxy)carbonyl>amino>-α-cyclohexanepropanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of *,S^*)>-β-<<(1,1-dimethylethoxy)carbonyl>amino>-α-cyclohexanepropanol

Chemical Property:

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Technology Process of *,S^*)>-β-<<(1,1-dimethylethoxy)carbonyl>amino>-α-cyclohexanepropanol

There total 3 articles about *,S^*)>-β-<<(1,1-dimethylethoxy)carbonyl>amino>-α-cyclohexanepropanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 37736-82-6
(S)-2-tert-butoxycarbonylamino-3-cyclohexylpropionic acid

: 151521-07-2
*,S^*)>-β-<<(1,1-dimethylethoxy)carbonyl>amino>-α-cyclohexanepropanol

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) 1,1'-carbonyldiimidazole, 2.) triethylamine / 1.) THF, 0 deg C, 30 min, 2.) THF, RT, 2.5 h

2: 85.8 percent / LiAlH₄ / tetrahydrofuran; diethyl ether / 0.5 h / 0 - 2 °C

3: 1.) BuLi / 1.) THF, -75 deg C, 20 min, 2.) THF, from -50 to -40 deg C, 3 h

With lithium aluminium tetrahydride; n-butyllithium; triethylamine; 1,1'-carbonyldiimidazole; In tetrahydrofuran; diethyl ether;
DOI:10.1021/jm00069a001

Reference yield:

: 115766-13-7
(S)-α-[[(1,1-dimethylethoxy)carbonyl]amino]-N-methoxy-N-methylcyclohexanepropanamide

: 151521-07-2
*,S^*)>-β-<<(1,1-dimethylethoxy)carbonyl>amino>-α-cyclohexanepropanol

Guidance literature:: Multi-step reaction with 2 steps

1: 85.8 percent / LiAlH₄ / tetrahydrofuran; diethyl ether / 0.5 h / 0 - 2 °C

2: 1.) BuLi / 1.) THF, -75 deg C, 20 min, 2.) THF, from -50 to -40 deg C, 3 h

With lithium aluminium tetrahydride; n-butyllithium; In tetrahydrofuran; diethyl ether;
DOI:10.1021/jm00069a001

Reference yield:

: 5418-86-0
tris(methylthio)methane

: 98105-42-1
(S)-2-(t-butoxycarbonylamino)-3-cyclohexyl-1-propanal

: 151521-07-2
*,S^*)>-β-<<(1,1-dimethylethoxy)carbonyl>amino>-α-cyclohexanepropanol

: *,R^*)>-β-<<(1,1-dimethylethoxy)carbonyl>amino>-α-cyclohexanepropanol

Guidance literature:: With n-butyllithium; Yield given. Multistep reaction; 1.) THF, -75 deg C, 20 min, 2.) THF, from -50 to -40 deg C, 3 h;
DOI:10.1021/jm00069a001