cis,trans-[Re(4,4'-dimethyl-2,2'-bipyridine)(CO)2(tris(4-methoxyphenyl)phosphine)(triisopropyl phosphite)]PF₆

Base Information

• Chemical Name: cis,trans-[Re(4,4'-dimethyl-2,2'-bipyridine)(CO)2(tris(4-methoxyphenyl)phosphine)(triisopropyl phosphite)]PF₆
• CAS No.: 870991-41-6
• Molecular Formula: C₄₄H₅₄N₂O₈P₂Re*F₆P
• Molecular Weight: 1132.04

Synonyms:cis,trans-[Re(4,4'-dimethyl-2,2'-bipyridine)(CO)2(tris(4-methoxyphenyl)phosphine)(triisopropyl phosphite)]PF₆

Chemical Property of cis,trans-[Re(4,4'-dimethyl-2,2'-bipyridine)(CO)2(tris(4-methoxyphenyl)phosphine)(triisopropyl phosphite)]PF₆

Chemical Property:

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Technology Process of cis,trans-[Re(4,4'-dimethyl-2,2'-bipyridine)(CO)2(tris(4-methoxyphenyl)phosphine)(triisopropyl phosphite)]PF₆

There total 1 articles about cis,trans-[Re(4,4'-dimethyl-2,2'-bipyridine)(CO)2(tris(4-methoxyphenyl)phosphine)(triisopropyl phosphite)]PF₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

ammonium hexafluorophosphate + cis,trans-[Re(4,4'-dimethyl-2,2'-bipyridine)(CO)2(tris(4-methoxyphenyl)phosphine)(triisopropyl phosphite)]CF3SO3 → cis,trans-[Re(4,4'-dimethyl-2,2'-bipyridine)(CO)2(tris(4-methoxyphenyl)phosphine)(triisopropyl phosphite)]PF6 (870991-41-6)

Guidance literature:

In methanol; dropwise addn. of a soln. of NH4PF6 in methanol to a soln. of rhenium complex in methanol; filtration, washing with water, drying in vac.; elem. anal.;

DOI:10.1021/ja053814u

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